(S)-N-(N-benzyl-N-(benzyloxycarbonyl)sulfamoyl)phenylalanine benzyl ester

Base Information

Chemical Name:(S)-N-(N-benzyl-N-(benzyloxycarbonyl)sulfamoyl)phenylalanine benzyl ester
CAS No.:478182-53-5
Molecular Formula:C₃₁H₃₀N₂O₆S
Molecular Weight:558.655
Hs Code.:

Synonyms:(S)-N-(N-benzyl-N-(benzyloxycarbonyl)sulfamoyl)phenylalanine benzyl ester

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Chemical Property of (S)-N-(N-benzyl-N-(benzyloxycarbonyl)sulfamoyl)phenylalanine benzyl ester

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Technology Process of (S)-N-(N-benzyl-N-(benzyloxycarbonyl)sulfamoyl)phenylalanine benzyl ester

There total 3 articles about (S)-N-(N-benzyl-N-(benzyloxycarbonyl)sulfamoyl)phenylalanine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 100-51-6,185532-71-2
benzyl alcohol

: 478182-49-9
(S)-N-(N-(benzyloxycarbonyl)sulfamoyl)phenylalanine benzyl ester

: 478182-53-5
(S)-N-(N-benzyl-N-(benzyloxycarbonyl)sulfamoyl)phenylalanine benzyl ester

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/jm020258v

Reference yield:

: 89979-13-5
benzyl N-chlorosulfonylcarbamate

: 478182-53-5
(S)-N-(N-benzyl-N-(benzyloxycarbonyl)sulfamoyl)phenylalanine benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 2 h / 20 °C

2: 93 percent / PPh₃; diisopropyl azodicarboxylate / CH₂Cl₂ / 1 h / 20 °C

With di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine; In dichloromethane; 2: Mitsunobu reaction;
DOI:10.1021/jm020258v

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 478182-53-5
(S)-N-(N-benzyl-N-(benzyloxycarbonyl)sulfamoyl)phenylalanine benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂ / 0.5 h / 0 °C

2: Et₃N / CH₂Cl₂ / 2 h / 20 °C

3: 93 percent / PPh₃; diisopropyl azodicarboxylate / CH₂Cl₂ / 1 h / 20 °C

With di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine; In dichloromethane; 3: Mitsunobu reaction;
DOI:10.1021/jm020258v