N²-(4-aminocyclohexyl)-N⁶-(4-bromobenzyl)-9-cyclopentyl-9H-purine-2,6-diamine

Base Information

Chemical Name:N²-(4-aminocyclohexyl)-N⁶-(4-bromobenzyl)-9-cyclopentyl-9H-purine-2,6-diamine
CAS No.:1448338-03-1
Molecular Formula:C₂₃H₃₀BrN₇
Molecular Weight:484.442
Hs Code.:

N<SUP>2</SUP>-(4-aminocyclohexyl)-N<SUP>6</SUP>-(4-bromobenzyl)-9-cyclopentyl-9H-purine-2,6-diamine

Synonyms:N²-(4-aminocyclohexyl)-N⁶-(4-bromobenzyl)-9-cyclopentyl-9H-purine-2,6-diamine

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Chemical Property of N²-(4-aminocyclohexyl)-N⁶-(4-bromobenzyl)-9-cyclopentyl-9H-purine-2,6-diamine

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Technology Process of N²-(4-aminocyclohexyl)-N⁶-(4-bromobenzyl)-9-cyclopentyl-9H-purine-2,6-diamine

There total 3 articles about N²-(4-aminocyclohexyl)-N⁶-(4-bromobenzyl)-9-cyclopentyl-9H-purine-2,6-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1448337-97-0
(4-bromobenzyl)(2-chloro-9-cyclopentyl-9H-purine-6-yl)amine

: 2615-25-0
trans-1,4-cyclohexyldiamine

: 1448338-03-1
N²-(4-aminocyclohexyl)-N⁶-(4-bromobenzyl)-9-cyclopentyl-9H-purine-2,6-diamine

Guidance literature:: at 160 ℃; for 12h; Sealed tube; Inert atmosphere;
DOI:10.1021/jm4006884

Reference yield:

: 211733-67-4
9-(cyclopentyl)-2,6-(dichloro)-9H-purine

: 1448338-03-1
N²-(4-aminocyclohexyl)-N⁶-(4-bromobenzyl)-9-cyclopentyl-9H-purine-2,6-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / propan-1-ol / 4 h / 120 °C / Sealed tube; Inert atmosphere

2: 12 h / 160 °C / Sealed tube; Inert atmosphere

With N-ethyl-N,N-diisopropylamine; In propan-1-ol;
DOI:10.1021/jm4006884

Reference yield:

: 5451-40-1
2,6 dichloropurine

: 1448338-03-1
N²-(4-aminocyclohexyl)-N⁶-(4-bromobenzyl)-9-cyclopentyl-9H-purine-2,6-diamine

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate; 2,2'-azobis(isobutyronitrile) / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / propan-1-ol / 4 h / 120 °C / Sealed tube; Inert atmosphere

3: 12 h / 160 °C / Sealed tube; Inert atmosphere

With 2,2'-azobis(isobutyronitrile); di-isopropyl azodicarboxylate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; propan-1-ol;
DOI:10.1021/jm4006884