C₁₃H₁₉Cl₃N₂Si

Base Information

• Chemical Name: C₁₃H₁₉Cl₃N₂Si
• CAS No.: 1338693-20-1
• Molecular Formula: C₁₃H₁₉Cl₃N₂Si
• Molecular Weight: 337.752
• Mol file: 1338693-20-1.mol

Synonyms:C₁₃H₁₉Cl₃N₂Si

Chemical Property of C₁₃H₁₉Cl₃N₂Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₃H₁₉Cl₃N₂Si

There total 1 articles about C₁₃H₁₉Cl₃N₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

lithium N,N’-diisopropyl-benzamidinate → C13H19Cl3N2Si (1338693-20-1)

Guidance literature:

With tetrachlorosilane; In diethyl ether; at -78 - 20 ℃; for 4h; Inert atmosphere;

DOI:10.1039/c1dt10898k

Reference yield: 47.0%

8-quinolinol (148-24-3,24804-14-6) + C13H19Cl3N2Si (1338693-20-1) → C22H25Cl2N3OSi (1338693-22-3)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃; for 19h; Inert atmosphere;

DOI:10.1039/c1dt10898k

Reference yield:

C13H19Cl3N2Si (1338693-20-1) → C22H25N9OSi (1338693-28-9)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 19 h / 20 °C / Inert atmosphere

2: trimethylsilylazide / acetonitrile / 17 h / 20 °C / Inert atmosphere

With trimethylsilylazide; triethylamine; In tetrahydrofuran; acetonitrile;

DOI:10.1039/c1dt10898k

Downstream raw materials:

C₂₂H₂₅Cl₂N₃OSi

C₂₂H₂₅N₉OSi

C₂₄H₂₅N₅O₃Si

C₂₄H₂₅N₅OS₂Si