Bis(4-tert-butoxycarbonylphenyl) ketone hydrazone

Base Information

Chemical Name:Bis(4-tert-butoxycarbonylphenyl) ketone hydrazone
CAS No.:174471-86-4
Molecular Formula:C₂₃H₂₈N₂O₄
Molecular Weight:396.486
Hs Code.:

Synonyms:Bis(4-tert-butoxycarbonylphenyl) ketone hydrazone

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Chemical Property of Bis(4-tert-butoxycarbonylphenyl) ketone hydrazone

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Technology Process of Bis(4-tert-butoxycarbonylphenyl) ketone hydrazone

There total 4 articles about Bis(4-tert-butoxycarbonylphenyl) ketone hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 145531-11-9
bis(4-tert-butoxycarbonylphenyl)methanone

: 174471-86-4
Bis(4-tert-butoxycarbonylphenyl) ketone hydrazone

Guidance literature:: With hydrazine dihydrochloride; hydrazine hydrate; In ethanol; Heating;
DOI:10.1039/p19960000063

Reference yield:

: 3988-03-2
bis(4-bromophenyl)methanone

: 174471-86-4
Bis(4-tert-butoxycarbonylphenyl) ketone hydrazone

Guidance literature:: Multi-step reaction with 4 steps

1: 35 percent / dimethylformamide / 24 h / 140 °C

2: 78 percent / aq. H₂SO₄ / Heating

3: 47 percent / DCC, DMAP / CH₂Cl₂ / Ambient temperature

4: 98 percent / N₂H₄*H₂O, N₂H₄*2HCl / ethanol / Heating

With dmap; hydrazine dihydrochloride; sulfuric acid; hydrazine hydrate; dicyclohexyl-carbodiimide; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/p19960000063

Reference yield:

: 964-68-1
4,4'-benzophenonedicarboxylic acid

: 174471-86-4
Bis(4-tert-butoxycarbonylphenyl) ketone hydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 47 percent / DCC, DMAP / CH₂Cl₂ / Ambient temperature

2: 98 percent / N₂H₄*H₂O, N₂H₄*2HCl / ethanol / Heating

With dmap; hydrazine dihydrochloride; hydrazine hydrate; dicyclohexyl-carbodiimide; In ethanol; dichloromethane;
DOI:10.1039/p19960000063