Technology Process of C14H16BNO4
There total 3 articles about C14H16BNO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tris-(dibenzylideneacetone)dipalladium(0); 1,6-bis(diphenylphosphino)hexane; silver carbonate;
In
tetrahydrofuran;
at 40 ℃;
for 24h;
Sealed tube;
Inert atmosphere;
DOI:10.1016/j.tet.2013.05.050
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: bromine / dichloromethane / 0.58 h / 0 - 23 °C / Inert atmosphere
1.2: 1 h / 23 °C / Inert atmosphere
2.1: tris-(dibenzylideneacetone)dipalladium(0); 1,6-bis(diphenylphosphino)hexane; silver carbonate / tetrahydrofuran / 24 h / 40 °C / Sealed tube; Inert atmosphere
With
tris-(dibenzylideneacetone)dipalladium(0); 1,6-bis(diphenylphosphino)hexane; bromine; silver carbonate;
In
tetrahydrofuran; dichloromethane;
2.1: |Suzuki-Miyaura Coupling;
DOI:10.1016/j.tet.2013.05.050
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: Trimethyl borate / tetrahydrofuran / 5.5 h / -78 - 23 °C / Inert atmosphere
1.2: 2.17 h / 105 - 115 °C / Inert atmosphere
2.1: bromine / dichloromethane / 0.58 h / 0 - 23 °C / Inert atmosphere
2.2: 1 h / 23 °C / Inert atmosphere
3.1: tris-(dibenzylideneacetone)dipalladium(0); 1,6-bis(diphenylphosphino)hexane; silver carbonate / tetrahydrofuran / 24 h / 40 °C / Sealed tube; Inert atmosphere
With
tris-(dibenzylideneacetone)dipalladium(0); Trimethyl borate; 1,6-bis(diphenylphosphino)hexane; bromine; silver carbonate;
In
tetrahydrofuran; dichloromethane;
3.1: |Suzuki-Miyaura Coupling;
DOI:10.1016/j.tet.2013.05.050
