p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-4-O-α-D-glucopyranosyl-β-D-glucopyranoside

Base Information

Chemical Name:p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-4-O-α-D-glucopyranosyl-β-D-glucopyranoside
CAS No.:86203-96-5
Molecular Formula:C₂₂H₂₉F₃N₂O₁₂
Molecular Weight:570.474
Hs Code.:

Synonyms:p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-4-O-α-D-glucopyranosyl-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-4-O-α-D-glucopyranosyl-β-D-glucopyranoside

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Technology Process of p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-4-O-α-D-glucopyranosyl-β-D-glucopyranoside

There total 5 articles about p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-4-O-α-D-glucopyranosyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 86203-95-4
p-trifluoroacetamidophenyl 2-acetamido-3,6-di-O-acetyl-2-deoxy-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-β-D-glucopyranoside

: 86203-96-5
p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-4-O-α-D-glucopyranosyl-β-D-glucopyranoside

Guidance literature:: With sodium methylate; In methanol;
DOI:10.1016/S0008-6215(00)90951-0

Reference yield:

: 2709-93-5
N-trifluoroacetyl-4-aminophenol

: 86203-96-5
p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-4-O-α-D-glucopyranosyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 38 percent / silver silicate, molecular sieves / nitromethane / 4 h / Ambient temperature

2: 1.) hydrogen / 1.) 10 percent Pd/C / 1.) ethanol, 400 kPa, overnight; 2.) methanol, r.t., overnight

3: 59 percent / 0.1 M sodium methoxide / methanol

With molecular sieve; silver silicate; hydrogen; sodium methylate; palladium on activated charcoal; In methanol; nitromethane;
DOI:10.1016/S0008-6215(00)90951-0

Reference yield:

: 86203-92-1
3,6-di-O-acetyl-2-azido-2-deoxy-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranosyl bromide

: 86203-96-5
p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-4-O-α-D-glucopyranosyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 38 percent / silver silicate, molecular sieves / nitromethane / 4 h / Ambient temperature

2: 1.) hydrogen / 1.) 10 percent Pd/C / 1.) ethanol, 400 kPa, overnight; 2.) methanol, r.t., overnight

3: 59 percent / 0.1 M sodium methoxide / methanol

With molecular sieve; silver silicate; hydrogen; sodium methylate; palladium on activated charcoal; In methanol; nitromethane;
DOI:10.1016/S0008-6215(00)90951-0