9,11-Dimethyl-4,6-bis(1-methylaethyl)-2,2-diphenyl-1,3-benzodioxolo<5,6-b><1,4>benzodioxin-7-ol

Base Information

• Chemical Name: 9,11-Dimethyl-4,6-bis(1-methylaethyl)-2,2-diphenyl-1,3-benzodioxolo<5,6-b><1,4>benzodioxin-7-ol
• CAS No.: 101958-87-6
• Molecular Formula: C₃₃H₃₂O₅
• Molecular Weight: 508.614

Synonyms:9,11-Dimethyl-4,6-bis(1-methylaethyl)-2,2-diphenyl-1,3-benzodioxolo<5,6-b><1,4>benzodioxin-7-ol

Chemical Property of 9,11-Dimethyl-4,6-bis(1-methylaethyl)-2,2-diphenyl-1,3-benzodioxolo<5,6-b><1,4>benzodioxin-7-ol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9,11-Dimethyl-4,6-bis(1-methylaethyl)-2,2-diphenyl-1,3-benzodioxolo<5,6-b><1,4>benzodioxin-7-ol

There total 4 articles about 9,11-Dimethyl-4,6-bis(1-methylaethyl)-2,2-diphenyl-1,3-benzodioxolo<5,6-b><1,4>benzodioxin-7-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

Methansulfonsaeure-<9,11-dimethyl-4,6-bis(1-methylaethyl)-2,2-diphenyl-1,3-benzodioxolo<5,6-b><1,4>benzodioxin-7-yl>ester (101958-79-6) → 9,11-Dimethyl-4,6-bis(1-methylaethyl)-2,2-diphenyl-1,3-benzodioxolo<5,6-b><1,4>benzodioxin-7-ol (101958-87-6)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 60 ℃; for 8h;

DOI:10.1002/hlca.19850680407

Reference yield:

Dichlorodiphenylmethane (2051-90-3) → 9,11-Dimethyl-4,6-bis(1-methylaethyl)-2,2-diphenyl-1,3-benzodioxolo<5,6-b><1,4>benzodioxin-7-ol (101958-87-6)

Guidance literature:

Multi-step reaction with 2 steps

1: α-pinene / CHCl3 / 1.) 80 deg C, 12 h; 2.) 100 deg C, 24 h

2: 93 percent / LiAlH₄ / tetrahydrofuran / 8 h / 60 °C

With lithium aluminium tetrahydride; Pinene; In tetrahydrofuran; chloroform;

DOI:10.1002/hlca.19850680407

Reference yield:

Methanesulfonic acid 7,8-dihydroxy-1,9-diisopropyl-4,6-dimethyl-dibenzo[1,4]dioxin-2-yl ester (101958-81-0) → 9,11-Dimethyl-4,6-bis(1-methylaethyl)-2,2-diphenyl-1,3-benzodioxolo<5,6-b><1,4>benzodioxin-7-ol (101958-87-6)

Guidance literature:

Multi-step reaction with 2 steps

1: α-pinene / CHCl3 / 1.) 80 deg C, 12 h; 2.) 100 deg C, 24 h

2: 93 percent / LiAlH₄ / tetrahydrofuran / 8 h / 60 °C

With lithium aluminium tetrahydride; Pinene; In tetrahydrofuran; chloroform;

DOI:10.1002/hlca.19850680407

upstream raw materials:

Methansulfonsaeure-<9,11-dimethyl-4,6-bis(1-methylaethyl)-2,2-diphenyl-1,3-benzodioxolo<5,6-b><1,4>benzodioxin-7-yl>ester

Dichlorodiphenylmethane

Methanesulfonic acid 7,8-dihydroxy-1,9-diisopropyl-4,6-dimethyl-dibenzo[1,4]dioxin-2-yl ester

Methansulfonsaeure-<4,6-dimethyl-1,9-bis(1-methylaethyl)-7,8-dioxo-7,8-dihydrobenzo<1,4>dioxin-2-yl>ester

Downstream raw materials:

3-Methylbutansaeure-<9,11-dimethyl-4,6-bis(1-methylaethyl)-2,2-diphenyl-1,3-benzodioxolo<5,6-b><1,4>benzodioxin-7-yl>ester

Ecklonochinon B

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