trans-[Pd(C₆F₅)Br(CH₃CN)2]

Base Information

Chemical Name:trans-[Pd(C₆F₅)Br(CH₃CN)2]
CAS No.:125475-73-2
Molecular Formula:C₁₀H₆BrF₅N₂Pd
Molecular Weight:435.487
Hs Code.:

trans-[Pd(C<sub>6</sub>F<sub>5</sub>)Br(CH<sub>3</sub>CN)2]

Synonyms:trans-[Pd(C₆F₅)Br(CH₃CN)2]

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Chemical Property of trans-[Pd(C₆F₅)Br(CH₃CN)2]

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Technology Process of trans-[Pd(C₆F₅)Br(CH₃CN)2]

There total 1 articles about trans-[Pd(C₆F₅)Br(CH₃CN)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: trans-(nBu4N)2{Pd2(μ-Br)2(C6F5)2Br2}

: silver perchlorate

: 125475-73-2
bis(acetonitrile)bromo(pentafluorophenyl)palladium(II)

Guidance literature:: In acetonitrile; byproducts: AgBr, (N(C4H9)4ClO4; stirring (45 min); filtn. of AgBr, evapn., sepn. of NBu4ClO4 on extn. (Et2O), evapn., addn. of MeCN, solidifying of oil on addn. of hexane, filtn., drying (air); elem. anal.;

Reference yield: 95.0%

: 125475-73-2
bis(acetonitrile)bromo(pentafluorophenyl)palladium(II)

: 1042933-50-5
As(C₆H₅)2(C₆Cl₂F₃)

: 1042933-45-8
trans-[Pd(C₆F₅)(As(3,5-dichloro-2,4,6-trifluorophenyl)Ph₂)2Br]

Guidance literature:: In diethyl ether; (N2) the complex was added to As(C6H5)2(C6H11) in diethyl ether, the soln. was stirred for 45 min; the solvent was removed, hexane was added, cooled to -18°C, filtered, vac.-dried; elem. anal.;
DOI:10.1021/om800264a

Reference yield: 90.0%

: 125475-73-2
bis(acetonitrile)bromo(pentafluorophenyl)palladium(II)

: 603-32-7
triphenyl-arsane

: {Pd2(μ-Br)2(C6F5)2(AsPh3)2}

Guidance literature:: In dichloromethane; soln. AsPh3 in CH2Cl2 was added dropwise at room temp. to stirred soln. (PdBr(C6F5)(NCMe)2) in CH2Cl2 and stirred for 10 min; solvent was evapd. to dryness, residue was triturated in EtOH, solid wasfiltered, washed with EtOH, and air-dried; elem. anal.;
DOI:10.1021/om030507t