{tetraethyl 4,4',4'',4'''-([10-(5-{[6-(1H-imidazol-1-yl)hexyl]oxy}-2-[(triisopropylsilyl)ethynyl]phenyl)porphyrin-5,15-diyl-κN21,κN22,κN23,κN24]bis[benzene-2,1,3-triylbis(oxy)])tetrabutanoato(2-)}zinc

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Chemical Name:{tetraethyl 4,4',4'',4'''-([10-(5-{[6-(1H-imidazol-1-yl)hexyl]oxy}-2-[(triisopropylsilyl)ethynyl]phenyl)porphyrin-5,15-diyl-κN21,κN22,κN23,κN24]bis[benzene-2,1,3-triylbis(oxy)])tetrabutanoato(2-)}zinc
CAS No.:1033224-37-1
Molecular Formula:C₈₂H₉₈N₆O₁₃SiZn
Molecular Weight:1469.19
Hs Code.:

{tetraethyl 4,4',4'',4'''-([10-(5-{[6-(1H-imidazol-1-yl)hexyl]oxy}-2-[(triisopropylsilyl)ethynyl]phenyl)porphyrin-5,15-diyl-κN21,κN22,κN23,κN24]bis[benzene-2,1,3-triylbis(oxy)])tetrabutanoato(2-)}zinc

Synonyms:{tetraethyl 4,4',4'',4'''-([10-(5-{[6-(1H-imidazol-1-yl)hexyl]oxy}-2-[(triisopropylsilyl)ethynyl]phenyl)porphyrin-5,15-diyl-κN21,κN22,κN23,κN24]bis[benzene-2,1,3-triylbis(oxy)])tetrabutanoato(2-)}zinc

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Chemical Property of {tetraethyl 4,4',4'',4'''-([10-(5-{[6-(1H-imidazol-1-yl)hexyl]oxy}-2-[(triisopropylsilyl)ethynyl]phenyl)porphyrin-5,15-diyl-κN21,κN22,κN23,κN24]bis[benzene-2,1,3-triylbis(oxy)])tetrabutanoato(2-)}zinc

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Technology Process of {tetraethyl 4,4',4'',4'''-([10-(5-{[6-(1H-imidazol-1-yl)hexyl]oxy}-2-[(triisopropylsilyl)ethynyl]phenyl)porphyrin-5,15-diyl-κN21,κN22,κN23,κN24]bis[benzene-2,1,3-triylbis(oxy)])tetrabutanoato(2-)}zinc

There total 1 articles about {tetraethyl 4,4',4'',4'''-([10-(5-{[6-(1H-imidazol-1-yl)hexyl]oxy}-2-[(triisopropylsilyl)ethynyl]phenyl)porphyrin-5,15-diyl-κN21,κN22,κN23,κN24]bis[benzene-2,1,3-triylbis(oxy)])tetrabutanoato(2-)}zinc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1033224-35-9
(((CH₃CH₂OOCCH₂CH₂CH₂O)2C₆H₃)2(((CH₃)2CH)3SiCC(HO)C₆H₃)C₂₀H₉N₄)Zn

: 126311-74-8
1-(6-bromohexyl)-1H-imidazole

: 1033224-37-1
(((CH₃CH₂OOCCH₂CH₂CH₂O)2C₆H₃)2(((CH₃)2CH)3SiCC(C₃H₃N₂(CH₂)6O)C₆H₃)C₂₀H₉N₄)Zn

Guidance literature:: With Cs₂CO₃; In N,N-dimethyl-formamide; treatment of porphyrin deriv. with imidazole deriv. in DMF in presence of Cs2CO3 at 20°C for 14 h;
DOI:10.1002/anie.200705180

Reference yield: 93.0%

: 1033224-37-1
(((CH₃CH₂OOCCH₂CH₂CH₂O)2C₆H₃)2(((CH₃)2CH)3SiCC(C₃H₃N₂(CH₂)6O)C₆H₃)C₂₀H₉N₄)Zn

: 1033224-39-3
(((CH₃CH₂OOCCH₂CH₂CH₂O)2C₆H₃)2(HCC(C₃H₃N₂(CH₂)6O)C₆H₃)C₂₀H₉N₄)Zn

Guidance literature:: With (CH₃CH₂CH₂CH₂)4NF; In tetrahydrofuran; treatment of porphyrin deriv. with fluoride salt in THF at 20°C for 40 min;
DOI:10.1002/anie.200705180