Technology Process of C13H14FN5
There total 9 articles about C13H14FN5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
water; potassium carbonate;
In
tetrahydrofuran; methanol;
at 40 ℃;
for 24h;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: ozone / dichloromethane / -78 °C
1.2: 1 h / -78 °C / Inert atmosphere
2.1: hydrogenchloride / methanol; 1,4-dioxane / 2 h / 20 °C
3.1: tetrahydrofuran / 20 h / 20 - 60 °C
4.1: N,N-dimethyl-formamide / 5 h / 80 °C
5.1: hydrazinium monoacetate / ethanol / 1 h / Reflux
6.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C
7.1: acetonitrile / 1 h / 0 °C
7.2: 17 h / 20 - 80 °C
7.3: 20 h / 20 °C
8.1: potassium carbonate; water / tetrahydrofuran; methanol / 24 h / 40 °C
With
hydrogenchloride; water; hydrazinium monoacetate; potassium carbonate; ozone; trifluoroacetic acid;
In
tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrazinium monoacetate / ethanol / 1 h / Reflux
2.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C
3.1: acetonitrile / 1 h / 0 °C
3.2: 17 h / 20 - 80 °C
3.3: 20 h / 20 °C
4.1: potassium carbonate; water / tetrahydrofuran; methanol / 24 h / 40 °C
With
water; hydrazinium monoacetate; potassium carbonate; trifluoroacetic acid;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; acetonitrile;