cis-1,3-dihydroxy-trans-5-azidocyclohexane

Base Information

Chemical Name:cis-1,3-dihydroxy-trans-5-azidocyclohexane
CAS No.:337361-53-2
Molecular Formula:C₆H₁₁N₃O₂
Molecular Weight:157.172
Hs Code.:

Synonyms:cis-1,3-dihydroxy-trans-5-azidocyclohexane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-1,3-dihydroxy-trans-5-azidocyclohexane

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Technology Process of cis-1,3-dihydroxy-trans-5-azidocyclohexane

There total 2 articles about cis-1,3-dihydroxy-trans-5-azidocyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 171419-88-8,337361-52-1
cis-1,3-dihydroxy-5-tosyloxycyclohexane

: 337361-53-2
cis-1,3-dihydroxy-trans-5-azidocyclohexane

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 70 ℃; for 16h;
DOI:10.1039/b503606b

Reference yield:

: 50409-12-6,13314-30-2
cis,cis-1,3,5-trihydroxycyclohexane

: 337361-53-2
cis-1,3-dihydroxy-trans-5-azidocyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran / 0.17 h / 40 °C

1.2: pyridine / tetrahydrofuran / 0.5 h / 40 °C

1.3: 70 percent / tetrahydrofuran / 15 h / 20 °C

2.1: 80 percent / sodium azide / dimethylformamide / 16 h / 70 °C

With n-butyllithium; sodium azide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/b503606b