11,23-bis((4'-(diethylamino)-2'-methylphenyl)imino)-26,28-dihydroxypentacyclo<19.3.1.1^3,7.1^9,13.1^15,19>-octacosa-1(24),3,5,7(28),9,12,15,17,19(26),21-decaene-25,27-dione

Base Information

• Chemical Name: 11,23-bis((4'-(diethylamino)-2'-methylphenyl)imino)-26,28-dihydroxypentacyclo<19.3.1.1^3,7.1^9,13.1^15,19>-octacosa-1(24),3,5,7(28),9,12,15,17,19(26),21-decaene-25,27-dione
• CAS No.: 148249-68-7
• Molecular Formula: C₅₀H₅₂N₄O₄
• Molecular Weight: 772.987

Synonyms:11,23-bis((4'-(diethylamino)-2'-methylphenyl)imino)-26,28-dihydroxypentacyclo<19.3.1.1^3,7.1^9,13.1^15,19>-octacosa-1(24),3,5,7(28),9,12,15,17,19(26),21-decaene-25,27-dione

Chemical Property of 11,23-bis((4'-(diethylamino)-2'-methylphenyl)imino)-26,28-dihydroxypentacyclo<19.3.1.1^3,7.1^9,13.1^15,19>-octacosa-1(24),3,5,7(28),9,12,15,17,19(26),21-decaene-25,27-dione

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Technology Process of 11,23-bis((4'-(diethylamino)-2'-methylphenyl)imino)-26,28-dihydroxypentacyclo<19.3.1.1^3,7.1^9,13.1^15,19>-octacosa-1(24),3,5,7(28),9,12,15,17,19(26),21-decaene-25,27-dione

There total 3 articles about 11,23-bis((4'-(diethylamino)-2'-methylphenyl)imino)-26,28-dihydroxypentacyclo<19.3.1.1^3,7.1^9,13.1^15,19>-octacosa-1(24),3,5,7(28),9,12,15,17,19(26),21-decaene-25,27-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

25,26,27,28-tetrakis(hydroxy)calix[4]arene (248590-47-8,74568-07-3) + 4-diethylamino-2-methylaniline hydrochloride (2051-79-8,54749-07-4) → 23-((4'-(diethylamino)-2'-methylphenyl)imino)-26,27,28-trihydroxypentacyclo<19.3.13,7.19,13.115,19>-octacosa-1(24),3,5,7(28),9,11,13(27),15,17,19(26),21-undecaen-25-one (139056-17-0) + 11,23-bis((4'-(diethylamino)-2'-methylphenyl)imino)-26,28-dihydroxypentacyclo<19.3.1.13,7.19,13.115,19>-octacosa-1(24),3,5,7(28),9,12,15,17,19(26),21-decaene-25,27-dione (148249-68-7) + 17,23-bis([4'-(diethylamino)-2'-methylphenyl]imino)-27,28-dihydroxypentacyclo[19.3.1.13,7.19,13.115,19]-octacosa-1(24),3,5,7(28),9,11,13(27),15,18,21-decaene-25,26-dione + 5,11,17,23-tetrakis([4'-(diethylamino)-2'-methylphenyl]imino)pentacyclo[19.3.1.13,7.19,13.115,19]-octacosa-1(24),3,6,9,12,15,18,21-octaene-25,26,27,28-tetraone

Guidance literature:

With sodium hydroxide; potassium hexacyanoferrate(III); In acetone; for 2h; Product distribution; Ambient temperature;

DOI:10.1021/jo951907w

Reference yield: 35.0%

25,26,27,28-tetrakis(hydroxy)calix[4]arene (248590-47-8,74568-07-3) + 4-diethylamino-2-methylaniline hydrochloride (2051-79-8,54749-07-4) → 11,23-bis((4'-(diethylamino)-2'-methylphenyl)imino)-26,28-dihydroxypentacyclo<19.3.1.13,7.19,13.115,19>-octacosa-1(24),3,5,7(28),9,12,15,17,19(26),21-decaene-25,27-dione (148249-68-7)

Guidance literature:

With sodium hydroxide; potassium hexacyanoferrate(III); Ambient temperature;

DOI:10.1039/c39930000305

Reference yield: 3.0%

25,26,27,28-tetrakis(hydroxy)calix[4]arene (248590-47-8,74568-07-3) + 4-diethylamino-2-methylaniline hydrochloride (2051-79-8,54749-07-4) → 11,23-bis((4'-(diethylamino)-2'-methylphenyl)imino)-26,28-dihydroxypentacyclo<19.3.1.13,7.19,13.115,19>-octacosa-1(24),3,5,7(28),9,12,15,17,19(26),21-decaene-25,27-dione (148249-68-7) + 17,23-bis([4'-(diethylamino)-2'-methylphenyl]imino)-27,28-dihydroxypentacyclo[19.3.1.13,7.19,13.115,19]-octacosa-1(24),3,5,7(28),9,11,13(27),15,18,21-decaene-25,26-dione + 5,11,17,23-tetrakis([4'-(diethylamino)-2'-methylphenyl]imino)pentacyclo[19.3.1.13,7.19,13.115,19]-octacosa-1(24),3,6,9,12,15,18,21-octaene-25,26,27,28-tetraone

Guidance literature:

With sodium hydroxide; potassium hexacyanoferrate(III); In acetone; for 4h; Ambient temperature;

DOI:10.1021/jo951907w

upstream raw materials:

25,26,27,28-tetrakis(hydroxy)calix[4]arene

4-diethylamino-2-methylaniline hydrochloride

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