3-carboxybenzylophosphonic acid

Base Information

Chemical Name:3-carboxybenzylophosphonic acid
CAS No.:142646-13-7
Molecular Formula:C₈H₉O₅P
Molecular Weight:216.13
Hs Code.:

Synonyms:3-carboxybenzylophosphonic acid

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Chemical Property of 3-carboxybenzylophosphonic acid

Chemical Property:

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Technology Process of 3-carboxybenzylophosphonic acid

There total 7 articles about 3-carboxybenzylophosphonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 96534-02-0
3-(diethyoxyphosphorylmethyl)benzoic acid methyl ester

: 142646-13-7
3-carboxybenzylophosphonic acid

Guidance literature:: With hydrogenchloride; In water; for 10h; Reflux;
DOI:10.1039/c3ra44614j

Reference yield:

: 1711-06-4
3-Methylbenzoyl chloride

: 142646-13-7
3-carboxybenzylophosphonic acid

Guidance literature:: Multi-step reaction with 4 steps

1: dichloromethane / 1.5 h / Reflux

2: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 2 h / Reflux

3: 1 h / 145 - 150 °C

4: hydrogenchloride / water / 10 h / Reflux

With hydrogenchloride; N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; dichloromethane; water;
DOI:10.1039/c3ra44614j

Reference yield:

: 1129-28-8
3-methoxycarbonylbenzyl bromide

: 142646-13-7
3-carboxybenzylophosphonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1 h / 145 - 150 °C

2: hydrogenchloride / water / 10 h / Reflux

With hydrogenchloride; In water;
DOI:10.1039/c3ra44614j