C₆₆H₉₂O₁₂Si

Base Information

Chemical Name:C₆₆H₉₂O₁₂Si
CAS No.:1264660-96-9
Molecular Formula:C₆₆H₉₂O₁₂Si
Molecular Weight:1105.53
Hs Code.:

C<sub>66</sub>H<sub>92</sub>O<sub>12</sub>Si

Synonyms:C₆₆H₉₂O₁₂Si

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Chemical Property of C₆₆H₉₂O₁₂Si

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Technology Process of C₆₆H₉₂O₁₂Si

There total 26 articles about C₆₆H₉₂O₁₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1264660-73-2
C₂₅H₄₀O₅Si

: 1264660-71-0
C₄₁H₅₂O₇

: 1264660-89-0
C₆₆H₉₂O₁₂Si

: 1264660-96-9
C₆₆H₉₂O₁₂Si

Guidance literature:: C₄₁H₅₂O₇; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at 0 ℃; for 1h;

C₂₅H₄₀O₅Si; In tetrahydrofuran; hexane; at -78 ℃; for 0.333333h;
DOI:10.1021/ol102925d

Reference yield:

: 1225339-83-2
C₂₇H₂₇O₇P

: 1264660-96-9
C₆₆H₉₂O₁₂Si

Guidance literature:: Multi-step reaction with 14 steps

1.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 0 °C

1.2: 1 h / 50 °C

2.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

2.2: 0 - 20 °C

3.1: diisobutylaluminium hydride / hexane; dichloromethane / 0 - 20 °C

3.2: 2.5 h

4.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

5.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 19 h / 20 °C / Molecular sieve

6.1: zinc trifluoromethanesulfonate / tetrahydrofuran / 20 °C

7.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 20 °C

7.2: 15 h

8.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -78 °C

9.1: n-heptane; dichloromethane / -78 - 0 °C

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

11.1: 2,6-dimethylpyridine / dichloromethane / -78 °C

12.1: dimethyl sulfoxide / 3 h / 20 - 80 °C

13.1: diethyl ether / -78 - 0 °C

14.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 1 h / 0 °C

14.2: 0.33 h / -78 °C

With 1H-imidazole; 2,6-dimethylpyridine; n-butyllithium; tetrapropylammonium perruthennate; dimethylsulfide borane complex; tetrabutyl ammonium fluoride; zinc trifluoromethanesulfonate; sodium hydride; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; diisopropylamine; 9-bora-bicyclo[3.3.1]nonane; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; hexane; n-heptane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil; 1.2: Suzuki-Miyaura coupling / 14.2: Aldol condensation;
DOI:10.1021/ol102925d

Reference yield:

: 1225339-88-7
C₄₃H₆₈O₇Si₂

: 1264660-96-9
C₆₆H₉₂O₁₂Si

Guidance literature:: Multi-step reaction with 13 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

1.2: 0 - 20 °C

2.1: diisobutylaluminium hydride / hexane; dichloromethane / 0 - 20 °C

2.2: 2.5 h

3.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

4.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 19 h / 20 °C / Molecular sieve

5.1: zinc trifluoromethanesulfonate / tetrahydrofuran / 20 °C

6.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 20 °C

6.2: 15 h

7.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -78 °C

8.1: n-heptane; dichloromethane / -78 - 0 °C

9.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

10.1: 2,6-dimethylpyridine / dichloromethane / -78 °C

11.1: dimethyl sulfoxide / 3 h / 20 - 80 °C

12.1: diethyl ether / -78 - 0 °C

13.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 1 h / 0 °C

13.2: 0.33 h / -78 °C

With 1H-imidazole; 2,6-dimethylpyridine; n-butyllithium; tetrapropylammonium perruthennate; dimethylsulfide borane complex; tetrabutyl ammonium fluoride; zinc trifluoromethanesulfonate; sodium hydride; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; hexane; n-heptane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil; 13.2: Aldol condensation;
DOI:10.1021/ol102925d