diethyl 6,6'-(1,4-phenylene)bis(2-oxo-4-p-tolylcyclohex-3-enecarboxylate)

Base Information

Chemical Name:diethyl 6,6'-(1,4-phenylene)bis(2-oxo-4-p-tolylcyclohex-3-enecarboxylate)
CAS No.:1316308-23-2
Molecular Formula:C₃₈H₃₈O₆
Molecular Weight:590.716
Hs Code.:

Synonyms:diethyl 6,6'-(1,4-phenylene)bis(2-oxo-4-p-tolylcyclohex-3-enecarboxylate)

Suppliers and Price of diethyl 6,6'-(1,4-phenylene)bis(2-oxo-4-p-tolylcyclohex-3-enecarboxylate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl 6,6'-(1,4-phenylene)bis(2-oxo-4-p-tolylcyclohex-3-enecarboxylate)

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Technology Process of diethyl 6,6'-(1,4-phenylene)bis(2-oxo-4-p-tolylcyclohex-3-enecarboxylate)

There total 2 articles about diethyl 6,6'-(1,4-phenylene)bis(2-oxo-4-p-tolylcyclohex-3-enecarboxylate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 146492-34-4,26483-82-9
1,4-bis-(3-oxo-3-p-tolyl-propenyl)-benzene

: 141-97-9
ethyl acetoacetate

: 1316308-23-2
diethyl 6,6'-(1,4-phenylene)bis(2-oxo-4-p-tolylcyclohex-3-enecarboxylate)

Guidance literature:: With sodium ethanolate; In ethanol; at 70 - 80 ℃; for 6h;
DOI:10.3109/14756366.2010.530263

Reference yield:

: 122-00-9
para-methylacetophenone

: 1316308-23-2
diethyl 6,6'-(1,4-phenylene)bis(2-oxo-4-p-tolylcyclohex-3-enecarboxylate)

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / ethanol / 4 h / 0 °C

2: sodium ethanolate / ethanol / 6 h / 70 - 80 °C

With sodium ethanolate; sodium hydroxide; In ethanol; 1: Claisen-Schmidt condensation;
DOI:10.3109/14756366.2010.530263