<3-(4'-methoxybenzyl)-1,2,3,4-tetrahydro-4-oxo-2-thioxoquinazolin-1-yl> acetic acid

Base Information

Chemical Name:<3-(4'-methoxybenzyl)-1,2,3,4-tetrahydro-4-oxo-2-thioxoquinazolin-1-yl> acetic acid
CAS No.:128650-84-0
Molecular Formula:C₁₈H₁₆N₂O₄S
Molecular Weight:356.402
Hs Code.:

Synonyms:<3-(4'-methoxybenzyl)-1,2,3,4-tetrahydro-4-oxo-2-thioxoquinazolin-1-yl> acetic acid

Suppliers and Price of <3-(4'-methoxybenzyl)-1,2,3,4-tetrahydro-4-oxo-2-thioxoquinazolin-1-yl> acetic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of <3-(4'-methoxybenzyl)-1,2,3,4-tetrahydro-4-oxo-2-thioxoquinazolin-1-yl> acetic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of <3-(4'-methoxybenzyl)-1,2,3,4-tetrahydro-4-oxo-2-thioxoquinazolin-1-yl> acetic acid

There total 5 articles about <3-(4'-methoxybenzyl)-1,2,3,4-tetrahydro-4-oxo-2-thioxoquinazolin-1-yl> acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 128650-83-9
ethyl <3-(4'-methoxybenzyl)-1,2,3,4-tetrahydro-4-oxo-2-thioxoquinazolin-1-yl> acetate

: 128650-84-0
<3-(4'-methoxybenzyl)-1,2,3,4-tetrahydro-4-oxo-2-thioxoquinazolin-1-yl> acetic acid

Guidance literature:: With hydrogenchloride; In water; acetic acid; for 8h; Heating;
DOI:10.1016/0223-5234(90)90019-Y

Reference yield:

: 57384-71-1
1-Ethoxycarbonylmethyl-2H-3,1-benzoxazine-2,4(1H)-dione

: 128650-84-0
<3-(4'-methoxybenzyl)-1,2,3,4-tetrahydro-4-oxo-2-thioxoquinazolin-1-yl> acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 50 percent / ethanol / 2 h / Heating

2: 81 percent / HCl / ethanol / 3 h / Heating

3: 35 percent / sulfur / 0.5 h / 180 °C

4: 50 percent / 37percent HCl / acetic acid; H₂O / 8 h / Heating

With hydrogenchloride; sulfur; In ethanol; water; acetic acid;
DOI:10.1016/0223-5234(90)90019-Y

Reference yield:

: 118-48-9
isatoic anhydride

: 128650-84-0
<3-(4'-methoxybenzyl)-1,2,3,4-tetrahydro-4-oxo-2-thioxoquinazolin-1-yl> acetic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NAH / 1.) N,N-dimethyl acetamide, RT, 1 h, 2.) RT, 12 h

2: 50 percent / ethanol / 2 h / Heating

3: 81 percent / HCl / ethanol / 3 h / Heating

4: 35 percent / sulfur / 0.5 h / 180 °C

5: 50 percent / 37percent HCl / acetic acid; H₂O / 8 h / Heating

With hydrogenchloride; sodium hydride; sulfur; In ethanol; water; acetic acid;
DOI:10.1016/0223-5234(90)90019-Y