(S)-2-((R)-2-Amino-4-benzyloxycarbonyl-butyrylamino)-4-methyl-pentanoic acid methyl ester; hydrochloride

Base Information

Chemical Name:(S)-2-((R)-2-Amino-4-benzyloxycarbonyl-butyrylamino)-4-methyl-pentanoic acid methyl ester; hydrochloride
CAS No.:122668-42-2
Molecular Formula:C₁₉H₂₈N₂O₅*ClH
Molecular Weight:400.903
Hs Code.:

Synonyms:(S)-2-((R)-2-Amino-4-benzyloxycarbonyl-butyrylamino)-4-methyl-pentanoic acid methyl ester; hydrochloride

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Chemical Property of (S)-2-((R)-2-Amino-4-benzyloxycarbonyl-butyrylamino)-4-methyl-pentanoic acid methyl ester; hydrochloride

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Technology Process of (S)-2-((R)-2-Amino-4-benzyloxycarbonyl-butyrylamino)-4-methyl-pentanoic acid methyl ester; hydrochloride

There total 10 articles about (S)-2-((R)-2-Amino-4-benzyloxycarbonyl-butyrylamino)-4-methyl-pentanoic acid methyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13574-13-5
Boc-Glu(OBzl)-OH

: 77302-66-0,122668-42-2
L-γ-O-benzylglutamyl-L-leucine methyl ester hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 92.2 percent / N-methylmorpholine, 1-hydroxybenzotriazole (HOBt), dicyclohexylcarbodiimide (DCC) / CH₂Cl₂ / 22 h / 0 - 20 °C

2: 4 N HCl / dioxane / 1 h / Ambient temperature

With 4-methyl-morpholine; hydrogenchloride; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In 1,4-dioxane; dichloromethane;
DOI:10.1021/jm00138a013

Reference yield:

: 7517-19-3
methyl (L)-leucinate hydrochloride

: 77302-66-0,122668-42-2
L-γ-O-benzylglutamyl-L-leucine methyl ester hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 92.2 percent / N-methylmorpholine, 1-hydroxybenzotriazole (HOBt), dicyclohexylcarbodiimide (DCC) / CH₂Cl₂ / 22 h / 0 - 20 °C

2: 4 N HCl / dioxane / 1 h / Ambient temperature

With 4-methyl-morpholine; hydrogenchloride; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In 1,4-dioxane; dichloromethane;
DOI:10.1021/jm00138a013