methyl 3,5-di-O-benzyl-2-O-(4-methylbenzoyl)-β-D-[2-2H1]arabinofuranoside

Base Information

Chemical Name:methyl 3,5-di-O-benzyl-2-O-(4-methylbenzoyl)-β-D-[2-2H1]arabinofuranoside
CAS No.:380883-52-3
Molecular Formula:C₂₈H₃₀O₆
Molecular Weight:463.535
Hs Code.:

Synonyms:methyl 3,5-di-O-benzyl-2-O-(4-methylbenzoyl)-β-D-[2-2H1]arabinofuranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3,5-di-O-benzyl-2-O-(4-methylbenzoyl)-β-D-[2-2H1]arabinofuranoside

Chemical Property:

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Technology Process of methyl 3,5-di-O-benzyl-2-O-(4-methylbenzoyl)-β-D-[2-2H1]arabinofuranoside

There total 3 articles about methyl 3,5-di-O-benzyl-2-O-(4-methylbenzoyl)-β-D-[2-2H1]arabinofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 874-60-2
4-methyl-benzoyl chloride

: (4R,5R)-4-Benzyloxy-5-benzyloxymethyl-2-methoxy-dihydro-furan-3-one

: 380883-52-3
methyl 3,5-di-O-benzyl-2-O-(4-methylbenzoyl)-β-D-[2-2H1]arabinofuranoside

: methyl 3,5-di-O-benzyl-2-O-(4-methylbenzoyl)-α-D-[2-2H1]ribofuranoside

Guidance literature:: (4R,5R)-4-Benzyloxy-5-benzyloxymethyl-2-methoxy-dihydro-furan-3-one; With lithium aluminium deuteride; In diethyl ether; at 20 ℃;

4-methyl-benzoyl chloride; With pyridine; at 20 ℃;
DOI:10.1002/hlca.200390062

Reference yield: 26.0%

: 874-60-2
4-methyl-benzoyl chloride

: C₂₀H₂₃⁽²⁾HO₅

: 380883-52-3
methyl 3,5-di-O-benzyl-2-O-(4-methylbenzoyl)-β-D-[2-2H1]arabinofuranoside

: methyl 3,5-di-O-benzyl-2-O-(4-methylbenzoyl)-α-D-[2-2H1]ribofuranoside

Guidance literature:: With pyridine; at 20 ℃;
DOI:10.1081/NCN-100002549

Reference yield:

: 55775-39-8
1-O-methyl-3,5-di-O-benzyl-D-ribofuranoside

: 874-60-2
4-methyl-benzoyl chloride

: 380883-52-3
methyl 3,5-di-O-benzyl-2-O-(4-methylbenzoyl)-β-D-[2-2H1]arabinofuranoside

: methyl 3,5-di-O-benzyl-2-O-(4-methylbenzoyl)-α-D-[2-2H1]ribofuranoside

Guidance literature:: 1-O-methyl-3,5-di-O-benzyl-D-ribofuranoside; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -70 ℃; for 4h;

With lithium aluminium deuteride; In diethyl ether; at 0 - 20 ℃;

4-methyl-benzoyl chloride; With pyridine; at 20 ℃;
DOI:10.1002/hlca.200490069