Dibenzyl 3,7-diethyl-5-methoxycarbonyl-2,8-dimethyldihydrodipyrrin-1,9-dicarboxylate

Base Information

Chemical Name:Dibenzyl 3,7-diethyl-5-methoxycarbonyl-2,8-dimethyldihydrodipyrrin-1,9-dicarboxylate
CAS No.:161690-41-1
Molecular Formula:C₃₃H₃₆N₂O₆
Molecular Weight:556.659
Hs Code.:

Synonyms:Dibenzyl 3,7-diethyl-5-methoxycarbonyl-2,8-dimethyldihydrodipyrrin-1,9-dicarboxylate

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Chemical Property of Dibenzyl 3,7-diethyl-5-methoxycarbonyl-2,8-dimethyldihydrodipyrrin-1,9-dicarboxylate

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Technology Process of Dibenzyl 3,7-diethyl-5-methoxycarbonyl-2,8-dimethyldihydrodipyrrin-1,9-dicarboxylate

There total 6 articles about Dibenzyl 3,7-diethyl-5-methoxycarbonyl-2,8-dimethyldihydrodipyrrin-1,9-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 16326-34-4
diethoxymethyl acetate

: 51089-83-9
benzyl 4-ethyl-3-methyl-1H-pyrrole-2-carboxylate

: 161690-41-1
Dibenzyl 3,7-diethyl-5-methoxycarbonyl-2,8-dimethyldihydrodipyrrin-1,9-dicarboxylate

Guidance literature:: With pyridinium p-toluenesulfonate; In toluene; at 120 ℃;

Reference yield: 60.0%

: 89-91-8
Methyl dimethoxyacetate

: 51089-83-9
benzyl 4-ethyl-3-methyl-1H-pyrrole-2-carboxylate

: 161690-41-1
Dibenzyl 3,7-diethyl-5-methoxycarbonyl-2,8-dimethyldihydrodipyrrin-1,9-dicarboxylate

Guidance literature:: With pyridinium p-toluenesulfonate; In toluene; at 120 ℃; for 228h;

Reference yield:

: 1925-61-7
benzyl 4-ethyl-3,5-dimethylpyrrole-2-carboxylate

: 161690-41-1
Dibenzyl 3,7-diethyl-5-methoxycarbonyl-2,8-dimethyldihydrodipyrrin-1,9-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: SO₂Cl₂

1.2: I₂; KI

1.3: Zn; AcOH

With sulfuryl dichloride;
DOI:10.1021/jo0100143