3-({1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}amino)-4-nitrobenzonitrile

Base Information

Chemical Name:3-({1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}amino)-4-nitrobenzonitrile
CAS No.:950772-82-4
Molecular Formula:C₂₀H₂₈N₄O₃
Molecular Weight:372.467
Hs Code.:

Synonyms:3-({1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}amino)-4-nitrobenzonitrile

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Chemical Property of 3-({1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}amino)-4-nitrobenzonitrile

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Technology Process of 3-({1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}amino)-4-nitrobenzonitrile

There total 1 articles about 3-({1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}amino)-4-nitrobenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 218632-01-0
3-fluoro-4-nitrobenzonitrile

: 1-[trans-4-(ethoxy)cyclohexyl]-4-piperidinamine dihydrochloride

: 950772-82-4
3-({1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}amino)-4-nitrobenzonitrile

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 - 70 ℃; for 6h;

Reference yield: 90.0%

: 950772-82-4
3-({1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}amino)-4-nitrobenzonitrile

: 950772-83-5
4-amino-3-({1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}amino)benzonitrile

Guidance literature:: With hydrogenchloride; iron; In ethanol; water; at 20 ℃; for 1.5h;

Reference yield:

: 950772-82-4
3-({1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}amino)-4-nitrobenzonitrile

: 3-{1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}-2-oxo-2,3-dihydro-1H-benzimidazole-5-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; iron / ethanol; water / 1.5 h / 20 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 °C

With hydrogenchloride; iron; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane; water;