3-[5-[[1-(benzyloxycarbonyl)-2(S)-azetidinyl]methoxy]-3-pyridyl]benzylamine

Base Information

Chemical Name:3-[5-[[1-(benzyloxycarbonyl)-2(S)-azetidinyl]methoxy]-3-pyridyl]benzylamine
CAS No.:1222138-89-7
Molecular Formula:C₂₄H₂₅N₃O₃
Molecular Weight:403.481
Hs Code.:

Synonyms:3-[5-[[1-(benzyloxycarbonyl)-2(S)-azetidinyl]methoxy]-3-pyridyl]benzylamine

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Chemical Property of 3-[5-[[1-(benzyloxycarbonyl)-2(S)-azetidinyl]methoxy]-3-pyridyl]benzylamine

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Technology Process of 3-[5-[[1-(benzyloxycarbonyl)-2(S)-azetidinyl]methoxy]-3-pyridyl]benzylamine

There total 1 articles about 3-[5-[[1-(benzyloxycarbonyl)-2(S)-azetidinyl]methoxy]-3-pyridyl]benzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.5%

: 1222138-84-2
tert-butyl [3-[5-[[1-(benzyloxycarbonyl)-2(S)-azetidinyl]methoxy]-3-pyridyl]benzyl]carbamate

: 1222138-89-7
3-[5-[[1-(benzyloxycarbonyl)-2(S)-azetidinyl]methoxy]-3-pyridyl]benzylamine

Guidance literature:: tert-butyl [3-[5-[[1-(benzyloxycarbonyl)-2(S)-azetidinyl]methoxy]-3-pyridyl]benzyl]carbamate; With water; trifluoroacetic acid; In dichloromethane; for 7h;

With ammonia; In methanol; pH=8 - 9;

Reference yield: 96.0%

: 1222138-89-7
3-[5-[[1-(benzyloxycarbonyl)-2(S)-azetidinyl]methoxy]-3-pyridyl]benzylamine

: 108-24-7
acetic anhydride

: 1222138-91-1
N-[3-[5-[[1-(benzyloxycarbonyl)-2(S)-azetidinyl]methoxy]-3-pyridyl]benzyl]acetamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; Cooling with ice;

Reference yield:

: 1222138-89-7
3-[5-[[1-(benzyloxycarbonyl)-2(S)-azetidinyl]methoxy]-3-pyridyl]benzylamine

: 1222135-00-3
N-[3-[5-[[2(S)-azetidinyl]methoxy]-3-pyridyl]benzyl]acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / methanol; dichloromethane / 2.5 h / 20 °C / Cooling with ice

2: palladium 10% on activated carbon; hydrogen / methanol; water / 2.75 h

With palladium 10% on activated carbon; hydrogen; triethylamine; In methanol; dichloromethane; water;