spiro

Base Information

• Chemical Name: spiro
• CAS No.: 56169-89-2
• Molecular Formula: C₁₁H₁₆S
• Molecular Weight: 180.314

Synonyms:spiro

Chemical Property of spiro

Chemical Property:

Purity/Quality:

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Technology Process of spiro

There total 2 articles about spiro which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

2',5'-dihydrospiro (31934-34-6) → 2-methylideneadamantane (875-72-9) + spiro (56169-89-2) + homoadamantane-2-thione (97462-11-8)

Guidance literature:

In xylene; at 80 ℃; for 30h;

DOI:10.1016/S0040-4039(00)98509-5

Reference yield: 16.0%

C11H16N2S (31934-34-6) → 2-methylideneadamantane (875-72-9) + homoadamantane-2-thione (97462-11-8) + C11H16S (56169-89-2)

Guidance literature:

In xylene; at 80 ℃; for 30h;

Reference yield: 91.0%

spiro (56169-89-2) + methyl α-cyano-4-nitrocinnamate → methyl 3'-cyano-4'-p-nitrophenylspiro[adamantane-2,2'-thiolane]-3'-carboxylate

Guidance literature:

In tetrahydrofuran; at 65 ℃; for 3h;

DOI:10.1002/jhet.5570360423

upstream raw materials:

2',5'-dihydrospiro

C₁₁H₁₆N₂S

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