[Mo(N₂)₂(2-(di-tert-butylphosphino)methyl-6-(diphenylphosphino)methylpyridine)]₂(μ-N₂)

Base Information

• Chemical Name: [Mo(N₂)₂(2-(di-tert-butylphosphino)methyl-6-(diphenylphosphino)methylpyridine)]₂(μ-N₂)
• CAS No.: 1415230-04-4
• Molecular Formula: C₅₄H₇₀Mo₂N₁₂P₄
• Molecular Weight: 1203.01

Synonyms:[Mo(N₂)₂(2-(di-tert-butylphosphino)methyl-6-(diphenylphosphino)methylpyridine)]₂(μ-N₂)

Chemical Property of [Mo(N₂)₂(2-(di-tert-butylphosphino)methyl-6-(diphenylphosphino)methylpyridine)]₂(μ-N₂)

Chemical Property:

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Technology Process of [Mo(N₂)₂(2-(di-tert-butylphosphino)methyl-6-(diphenylphosphino)methylpyridine)]₂(μ-N₂)

There total 3 articles about [Mo(N₂)₂(2-(di-tert-butylphosphino)methyl-6-(diphenylphosphino)methylpyridine)]₂(μ-N₂) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

[MoCl3(2-(di-tert-butylphosphino)methyl-6-(diphenylphosphino)methylpyridine)] (1415230-00-0) + nitrogen (7727-37-9) → [Mo(N2)2(2-(di-tert-butylphosphino)methyl-6-(diphenylphosphino)methylpyridine)]2(μ-N2) (1415230-04-4)

Guidance literature:

With 0.5 wt% Na-Hg; In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere; Schlenk technique;

DOI:10.1021/om301046t

Reference yield:

2-methyl-6-((diphenylphosphino)methyl)pyridine (60398-58-5) → [Mo(N2)2(2-(di-tert-butylphosphino)methyl-6-(diphenylphosphino)methylpyridine)]2(μ-N2) (1415230-04-4)

Guidance literature:

Multi-step reaction with 3 steps

1.1: n-butyllithium / diethyl ether; hexane / 15 h / Reflux; Inert atmosphere; Schlenk technique

1.2: 6 h / 20 °C / Inert atmosphere; Schlenk technique

2.1: tetrahydrofuran / 20 h / 50 °C / Inert atmosphere; Schlenk technique

3.1: 0.5 wt% Na-Hg / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere; Schlenk technique

With n-butyllithium; 0.5 wt% Na-Hg; In tetrahydrofuran; diethyl ether; hexane;

DOI:10.1021/om301046t

Reference yield:

2-(di-tert-butylphosphino)methyl-6-(diphenylphosphino)methylpyridine (1415229-96-7) → [Mo(N2)2(2-(di-tert-butylphosphino)methyl-6-(diphenylphosphino)methylpyridine)]2(μ-N2) (1415230-04-4)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / 20 h / 50 °C / Inert atmosphere; Schlenk technique

2: 0.5 wt% Na-Hg / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere; Schlenk technique

With 0.5 wt% Na-Hg; In tetrahydrofuran;

DOI:10.1021/om301046t

upstream raw materials:

2-methyl-6-((diphenylphosphino)methyl)pyridine

2-(di-tert-butylphosphino)methyl-6-(diphenylphosphino)methylpyridine

[MoCl₃(2-(di-tert-butylphosphino)methyl-6-(diphenylphosphino)methylpyridine)]

nitrogen

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