C₇₂H₁₀₂O₁₉Si₂

Base Information

Chemical Name:C₇₂H₁₀₂O₁₉Si₂
CAS No.:198124-48-0
Molecular Formula:C₇₂H₁₀₂O₁₉Si₂
Molecular Weight:1327.76
Hs Code.:

C<sub>72</sub>H<sub>102</sub>O<sub>19</sub>Si<sub>2</sub>

Synonyms:C₇₂H₁₀₂O₁₉Si₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₇₂H₁₀₂O₁₉Si₂

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Technology Process of C₇₂H₁₀₂O₁₉Si₂

There total 10 articles about C₇₂H₁₀₂O₁₉Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 198124-77-5
C₇₂H₁₀₄O₁₉Si₂

: 198124-48-0
C₇₂H₁₀₂O₁₉Si₂

Guidance literature:: With Dess-Martin periodane;
DOI:10.1021/ja971828x

Reference yield:

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 198124-48-0
C₇₂H₁₀₂O₁₉Si₂

Guidance literature:: Multi-step reaction with 6 steps

1: DEAD, PPh₃ / tetrahydrofuran

2: Et₃N, HF / acetonitrile

3: NBS / CHCl₃

4: DIPEA / CH₂Cl₂

5: 1.) n-BuLi / 1.) THF, -100 deg C

6: 94 percent / Dess-Martin periodinane

With N-Bromosuccinimide; n-butyllithium; hydrogen fluoride; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; chloroform; acetonitrile;
DOI:10.1021/ja971828x

Reference yield:

: 198124-44-6
5-allyloxy-3-bromo-7-methoxymethoxy-2,6-dimethyl-[1,4]-naphthoquinone

: 198124-48-0
C₇₂H₁₀₂O₁₉Si₂

Guidance literature:: Multi-step reaction with 9 steps

1: imidazole / dimethylformamide

2: 1.) Na₂S₂O₄, adogen 464, 2.) NaOH / 1.) CH₂Cl₂, H₂O, 2.) CH₂Cl₂, H₂O

3: 1.) n-BuLi / 1.) THF, -78 deg C

4: DEAD, PPh₃ / tetrahydrofuran

5: Et₃N, HF / acetonitrile

6: NBS / CHCl₃

7: DIPEA / CH₂Cl₂

8: 1.) n-BuLi / 1.) THF, -100 deg C

9: 94 percent / Dess-Martin periodinane

With 1H-imidazole; sodium hydroxide; N-Bromosuccinimide; n-butyllithium; sodium dithionite; adogen 464; hydrogen fluoride; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; chloroform; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja971828x