C₈₇H₁₆₈O₉Si₃

Base Information

• Chemical Name: C₈₇H₁₆₈O₉Si₃
• CAS No.: 1616796-92-9
• Molecular Formula: C₈₇H₁₆₈O₉Si₃
• Molecular Weight: 1442.54
• Mol file: 1616796-92-9.mol

Synonyms:C₈₇H₁₆₈O₉Si₃

Chemical Property of C₈₇H₁₆₈O₉Si₃

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₈₇H₁₆₈O₉Si₃

There total 1 articles about C₈₇H₁₆₈O₉Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

benzene-1,3,5-tricarboxylic acid (554-95-0) + 1-((tert-butyldimethylsilyl)oxy)-20-eicosandiol (1616796-91-8) → C87H168O9Si3 (1616796-92-9)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In chloroform; for 42h;

DOI:10.1021/ja504891x

Reference yield: 98.0%

C87H168O9Si3 (1616796-92-9) → C69H126O9 (1616796-93-0)

Guidance literature:

With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; at 50 ℃; for 8h;

DOI:10.1021/ja504891x

Reference yield:

C87H168O9Si3 (1616796-92-9) → C72H123F9O15S3 (1616796-89-4)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid; tetrabutyl ammonium fluoride / tetrahydrofuran / 8 h / 50 °C

2: poly(4-vinylpyridine) / dichloromethane / 2 h / Reflux

With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ja504891x

upstream raw materials:

benzene-1,3,5-tricarboxylic acid

1-((tert-butyldimethylsilyl)oxy)-20-eicosandiol

Downstream raw materials:

C₇₂H₁₂₃F₉O₁₅S₃

C₆₉H₁₂₆O₉