C₃₁H₃₂NOP

Base Information

• Chemical Name: C₃₁H₃₂NOP
• CAS No.: 1324393-17-0
• Molecular Formula: C₃₁H₃₂NOP
• Molecular Weight: 465.575
• Mol file: 1324393-17-0.mol

Synonyms:C₃₁H₃₂NOP

Chemical Property of C₃₁H₃₂NOP

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₁H₃₂NOP

There total 5 articles about C₃₁H₃₂NOP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

C19H15OP (1324393-16-9) + 2,6-diisopropyl-1-azidobenzene (136551-45-6) → C31H32NOP (1324393-17-0)

Guidance literature:

In benzene; at 20 ℃; for 12h; Inert atmosphere;

DOI:10.1021/ic201139b

Reference yield:

(-)-(o-menthyl)chlorophenylphosphine → C31H32NOP (1324393-17-0)

Guidance literature:

Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 - 20 °C / Inert atmosphere

1.2: 10 h / -78 - 20 °C / Inert atmosphere

1.3: 1 h / 0 - 20 °C / Inert atmosphere

2.1: diethyl ether; benzene / 10 h / 20 °C / Inert atmosphere

3.1: diethylamine / 10 h / 40 °C / Inert atmosphere

4.1: benzene / 12 h / 20 °C / Inert atmosphere

With n-butyllithium; diethylamine; In tetrahydrofuran; diethyl ether; hexane; benzene;

DOI:10.1021/ic201139b

Reference yield:

Dichlorophenylphosphine (644-97-3) → C31H32NOP (1324393-17-0)

Guidance literature:

Multi-step reaction with 5 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0 °C / Inert atmosphere

1.2: 15 h / -78 - 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 - 20 °C / Inert atmosphere

2.2: 10 h / -78 - 20 °C / Inert atmosphere

2.3: 1 h / 0 - 20 °C / Inert atmosphere

3.1: diethyl ether; benzene / 10 h / 20 °C / Inert atmosphere

4.1: diethylamine / 10 h / 40 °C / Inert atmosphere

5.1: benzene / 12 h / 20 °C / Inert atmosphere

With n-butyllithium; diethylamine; In tetrahydrofuran; diethyl ether; hexane; benzene;

DOI:10.1021/ic201139b

upstream raw materials:

4-(BH₃)PPhMe-dbf

C₁₉H₁₅OP

2,6-diisopropyl-1-azidobenzene

Dichlorophenylphosphine