Technology Process of C24H33N3O
There total 10 articles about C24H33N3O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate;
In
N,N-dimethyl-formamide;
at 80 ℃;
Inert atmosphere;
DOI:10.1016/j.bmc.2012.11.042
- Guidance literature:
-
Multi-step reaction with 6 steps
1: hydrogen; triethylamine / methanol; water / 13.5 h / 20 °C / Inert atmosphere
2: tetra-(n-butyl)ammonium iodide; potassium tert-butylate / 0.08 h / -20 °C
3: hydrogen; palladium 10% on activated carbon / 1,4-dioxane / 16 h / 20 °C / Inert atmosphere
4: hydrogenchloride / water; 1,4-dioxane / 3 h / 20 °C
5: pyridine iodine monochloride / water; dichloromethane / 6.5 h / 20 °C
6: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate / N,N-dimethyl-formamide / 80 °C / Inert atmosphere
With
hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; palladium 10% on activated carbon; potassium tert-butylate; hydrogen; pyridine iodine monochloride; tetra-(n-butyl)ammonium iodide; triethylamine;
In
1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;
6: |Suzuki Coupling;
DOI:10.1016/j.bmc.2012.11.042
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogen; palladium 10% on activated carbon / 1,4-dioxane / 16 h / 20 °C / Inert atmosphere
2: hydrogenchloride / water; 1,4-dioxane / 3 h / 20 °C
3: pyridine iodine monochloride / water; dichloromethane / 6.5 h / 20 °C
4: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate / N,N-dimethyl-formamide / 80 °C / Inert atmosphere
With
hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; palladium 10% on activated carbon; hydrogen; pyridine iodine monochloride;
In
1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;
4: |Suzuki Coupling;
DOI:10.1016/j.bmc.2012.11.042
