C₂₂H₂₃N₃O₃

Base Information

Chemical Name:C₂₂H₂₃N₃O₃
CAS No.:1279090-81-1
Molecular Formula:C₂₂H₂₃N₃O₃
Molecular Weight:377.443
Hs Code.:

C<sub>22</sub>H<sub>23</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:C₂₂H₂₃N₃O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₃N₃O₃

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Technology Process of C₂₂H₂₃N₃O₃

There total 7 articles about C₂₂H₂₃N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1279093-44-5
C₂₂H₂₄ClN₃O₃

: 1279090-81-1
C₂₂H₂₃N₃O₃

Guidance literature:: With potassium carbonate; 1,1'-bis(di-tertbutylphosphino)ferrocene; palladium diacetate; In 1-methyl-pyrrolidin-2-one; at 130 ℃;

Reference yield:

: 137553-42-5
2-fluoro-4-iodo-benzonitrile

: 1279090-81-1
C₂₂H₂₃N₃O₃

Guidance literature:: Multi-step reaction with 4 steps

1: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 2 h / 150 °C

2: sodium hydroxide; water; dihydrogen peroxide / dimethyl sulfoxide; methanol / 4 h / 20 °C

3: triethylamine / copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 1 h / 50 °C

4: potassium carbonate / palladium diacetate; 1,1'-bis(di-tertbutylphosphino)ferrocene / 1-methyl-pyrrolidin-2-one / 130 °C

With water; dihydrogen peroxide; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 1,1'-bis(di-tertbutylphosphino)ferrocene; palladium diacetate; In 1-methyl-pyrrolidin-2-one; methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 95-51-2
o-chloroaniline

: 1279090-81-1
C₂₂H₂₃N₃O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / tetrahydrofuran / 1 h / 20 °C

1.2: 2 h / Reflux

2.1: triethylamine / copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 1 h / 50 °C

3.1: potassium carbonate / palladium diacetate; 1,1'-bis(di-tertbutylphosphino)ferrocene / 1-methyl-pyrrolidin-2-one / 130 °C

With oxalyl dichloride; potassium carbonate; triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 1,1'-bis(di-tertbutylphosphino)ferrocene; palladium diacetate; N,N-dimethyl-formamide; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; N,N-dimethyl-formamide;