(2S)-2-4-(N-Boc-N-2-picolyl aminomethyl) benzoyl-5-((5,6,7,8-tetrahydroquinolin-8-yl) amino) valerate 1-naphthalenemethylamide

Base Information

Chemical Name:(2S)-2-4-(N-Boc-N-2-picolyl aminomethyl) benzoyl-5-((5,6,7,8-tetrahydroquinolin-8-yl) amino) valerate 1-naphthalenemethylamide
CAS No.:369656-15-5
Molecular Formula:C₄₄H₅₀N₆O₄
Molecular Weight:726.919
Hs Code.:

Synonyms:(2S)-2-4-(N-Boc-N-2-picolyl aminomethyl) benzoyl-5-((5,6,7,8-tetrahydroquinolin-8-yl) amino) valerate 1-naphthalenemethylamide

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Chemical Property of (2S)-2-4-(N-Boc-N-2-picolyl aminomethyl) benzoyl-5-((5,6,7,8-tetrahydroquinolin-8-yl) amino) valerate 1-naphthalenemethylamide

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Technology Process of (2S)-2-4-(N-Boc-N-2-picolyl aminomethyl) benzoyl-5-((5,6,7,8-tetrahydroquinolin-8-yl) amino) valerate 1-naphthalenemethylamide

There total 1 articles about (2S)-2-4-(N-Boc-N-2-picolyl aminomethyl) benzoyl-5-((5,6,7,8-tetrahydroquinolin-8-yl) amino) valerate 1-naphthalenemethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Nα-4-(N-Boc-N-2-picolylaminomethyl)benzoyl-(Nδ-2-chlorobenzyloxycarbonyl)-L-ornithine 1-naphthalenemethylamide

: 56826-69-8
5,6,7,8-tetrahydro-8-quinolinone

: 369656-15-5
(2S)-2-4-(N-Boc-N-2-picolyl aminomethyl) benzoyl-5-((5,6,7,8-tetrahydroquinolin-8-yl) amino) valerate 1-naphthalenemethylamide

Guidance literature:: Nα-4-(N-Boc-N-2-picolylaminomethyl)benzoyl-(Nδ-2-chlorobenzyloxycarbonyl)-L-ornithine 1-naphthalenemethylamide; With hydrogen; palladium 10% on activated carbon; In methanol; under 2280.15 Torr;

5,6,7,8-tetrahydro-8-quinolinone; In methanol; at 20 ℃; for 1h;

With sodium tetrahydroborate; In methanol; at 0 - 20 ℃; for 0.5h;

Reference yield:

: 369656-15-5
(2S)-2-4-(N-Boc-N-2-picolyl aminomethyl) benzoyl-5-((5,6,7,8-tetrahydroquinolin-8-yl) amino) valerate 1-naphthalenemethylamide

: (2S)-2-(4-(N-2-picolylaminomethyl)benzoylamino)-5-((5,6,7,8-tetrahydroquinolin-8-yl) amino) valerate 1-naphthalene methylamide hydrochloride

Guidance literature:: (2S)-2-4-(N-Boc-N-2-picolyl aminomethyl) benzoyl-5-((5,6,7,8-tetrahydroquinolin-8-yl) amino) valerate 1-naphthalenemethylamide; With hydrogenchloride; In 1,4-dioxane; methanol; at 20 ℃; for 2h;

With hydrogenchloride; In water;