13-benzoyl-12-(3,4-dimethoxyphenyl)-5,11,12,12a,13,14-hexahydro[1,5]benzo diazepino[2,3-b][1,4]benzodiazepin-14-one

Base Information

• Chemical Name: 13-benzoyl-12-(3,4-dimethoxyphenyl)-5,11,12,12a,13,14-hexahydro[1,5]benzo diazepino[2,3-b][1,4]benzodiazepin-14-one
• CAS No.: 1357572-39-4
• Molecular Formula: C₃₁H₂₆N₄O₄
• Molecular Weight: 518.572

Synonyms:13-benzoyl-12-(3,4-dimethoxyphenyl)-5,11,12,12a,13,14-hexahydro[1,5]benzo diazepino[2,3-b][1,4]benzodiazepin-14-one

Chemical Property of 13-benzoyl-12-(3,4-dimethoxyphenyl)-5,11,12,12a,13,14-hexahydro[1,5]benzo diazepino[2,3-b][1,4]benzodiazepin-14-one

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Technology Process of 13-benzoyl-12-(3,4-dimethoxyphenyl)-5,11,12,12a,13,14-hexahydro[1,5]benzo diazepino[2,3-b][1,4]benzodiazepin-14-one

There total 3 articles about 13-benzoyl-12-(3,4-dimethoxyphenyl)-5,11,12,12a,13,14-hexahydro[1,5]benzo diazepino[2,3-b][1,4]benzodiazepin-14-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

C25H20N2O5 (1357571-95-9) + 1,2-diamino-benzene (95-54-5) → C31H24N4O3 (1357572-13-4) + 13-benzoyl-12-(3,4-dimethoxyphenyl)-5,11,12,12a,13,14-hexahydro[1,5]benzo diazepino[2,3-b][1,4]benzodiazepin-14-one (1357572-39-4)

Guidance literature:

With sodium hydroxide; In water; N,N-dimethyl-formamide;

DOI:10.1002/jhet.756

Reference yield:

anthranilic acid amide (28144-70-9,88-68-6) → C31H24N4O3 (1357572-13-4) + 13-benzoyl-12-(3,4-dimethoxyphenyl)-5,11,12,12a,13,14-hexahydro[1,5]benzo diazepino[2,3-b][1,4]benzodiazepin-14-one (1357572-39-4)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid / benzene / Reflux

2: sodium hydroxide / water; N,N-dimethyl-formamide

With acetic acid; sodium hydroxide; In water; N,N-dimethyl-formamide; benzene;

DOI:10.1002/jhet.756

Reference yield:

2-phenyl-4-veratryliden-4H-oxazol-5-one (5415-56-5,25349-37-5,25349-38-6) → C31H24N4O3 (1357572-13-4) + 13-benzoyl-12-(3,4-dimethoxyphenyl)-5,11,12,12a,13,14-hexahydro[1,5]benzo diazepino[2,3-b][1,4]benzodiazepin-14-one (1357572-39-4)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid / benzene / Reflux

2: sodium hydroxide / water; N,N-dimethyl-formamide

With acetic acid; sodium hydroxide; In water; N,N-dimethyl-formamide; benzene;

DOI:10.1002/jhet.756

upstream raw materials:

C₂₅H₂₀N₂O₅

1,2-diamino-benzene

2-phenyl-4-veratryliden-4H-oxazol-5-one

anthranilic acid amide

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