2-(benzyloxy)phenoxy acetic acid <2-(2,6-dimethoxyphenoxy)ethyl>amide

Base Information

Chemical Name:2-(benzyloxy)phenoxy acetic acid <2-(2,6-dimethoxyphenoxy)ethyl>amide
CAS No.:244123-13-5
Molecular Formula:C₂₅H₂₇NO₆
Molecular Weight:437.492
Hs Code.:

Synonyms:2-(benzyloxy)phenoxy acetic acid <2-(2,6-dimethoxyphenoxy)ethyl>amide

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Chemical Property of 2-(benzyloxy)phenoxy acetic acid <2-(2,6-dimethoxyphenoxy)ethyl>amide

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Technology Process of 2-(benzyloxy)phenoxy acetic acid <2-(2,6-dimethoxyphenoxy)ethyl>amide

There total 3 articles about 2-(benzyloxy)phenoxy acetic acid <2-(2,6-dimethoxyphenoxy)ethyl>amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6272-38-4
O-benzylcatechol

: 244123-13-5
2-(benzyloxy)phenoxy acetic acid <2-(2,6-dimethoxyphenoxy)ethyl>amide

Guidance literature:: Multi-step reaction with 3 steps

1: 47 percent / K₂CO₃ / acetone / 8 h / Heating

2: 83 percent / 2 N aq. NAOH / 0.5 h / 70 °C

3: 1.) EtOCOCl, Et₃N / 1.) CHCl₃, 30 min, 2) CHCl₃, RT 4 h

With sodium hydroxide; chloroformic acid ethyl ester; potassium carbonate; triethylamine; In acetone;
DOI:10.1021/jm9910324

Reference yield:

: 244123-11-3
2-(benzyloxy)phenoxyacetic acid methyl ester

: 244123-13-5
2-(benzyloxy)phenoxy acetic acid <2-(2,6-dimethoxyphenoxy)ethyl>amide

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / 2 N aq. NAOH / 0.5 h / 70 °C

2: 1.) EtOCOCl, Et₃N / 1.) CHCl₃, 30 min, 2) CHCl₃, RT 4 h

With sodium hydroxide; chloroformic acid ethyl ester; triethylamine;
DOI:10.1021/jm9910324

Reference yield:

: 40515-98-8
2-(2,6-dimethoxyphenoxy)ethylamine

: 244123-12-4
2-(2-(benzyloxy)phenoxy)acetic acid

: 244123-13-5
2-(benzyloxy)phenoxy acetic acid <2-(2,6-dimethoxyphenoxy)ethyl>amide

Guidance literature:: With chloroformic acid ethyl ester; triethylamine; Yield given; Multistep reaction; 1.) CHCl₃, 30 min, 2) CHCl₃, RT 4 h;
DOI:10.1021/jm9910324