3-(benzyloxy)-N-hydroxybenzene carboximidoyl chloride

Base Information

Chemical Name:3-(benzyloxy)-N-hydroxybenzene carboximidoyl chloride
CAS No.:1062547-93-6
Molecular Formula:C₁₄H₁₂ClNO₂
Molecular Weight:261.708
Hs Code.:

Synonyms:3-(benzyloxy)-N-hydroxybenzene carboximidoyl chloride

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Chemical Property of 3-(benzyloxy)-N-hydroxybenzene carboximidoyl chloride

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Technology Process of 3-(benzyloxy)-N-hydroxybenzene carboximidoyl chloride

There total 5 articles about 3-(benzyloxy)-N-hydroxybenzene carboximidoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 93033-58-0
3-(benzyloxy)benzaldehyde oxime

: 1062547-93-6
3-(benzyloxy)-N-hydroxybenzene carboximidoyl chloride

Guidance literature:: With pyridine; N-chloro-succinimide; In tetrahydrofuran; at 60 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.bmcl.2008.07.047

Reference yield:

: (E)-1-(3-(benzyloxy)phenyl)-N-hydroxymethanimine

: 1062547-93-6
3-(benzyloxy)-N-hydroxybenzene carboximidoyl chloride

Guidance literature:: With N-chloro-succinimide; In N,N-dimethyl-formamide; at 10 - 35 ℃; for 4h;

Reference yield:

: 1700-37-4
3-Benzyloxybenzaldehyde

: 1062547-93-6
3-(benzyloxy)-N-hydroxybenzene carboximidoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride; sodium hydrogencarbonate / ethanol / 2 h / 50 °C

2: N-chloro-succinimide / N,N-dimethyl-formamide / 3.33 h / 20 - 35 °C

With N-chloro-succinimide; hydroxylamine hydrochloride; sodium hydrogencarbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2021.127979