2-{5-[4-(4-isopropyl-piperazin-1-ylmethyl)-phenyl]-[2,2';4',3'']terpyridin-6'-yl}-propan-2-ol

Base Information

Chemical Name:2-{5-[4-(4-isopropyl-piperazin-1-ylmethyl)-phenyl]-[2,2';4',3'']terpyridin-6'-yl}-propan-2-ol
CAS No.:1171041-31-8
Molecular Formula:C₃₂H₃₇N₅O
Molecular Weight:507.679
Hs Code.:

Synonyms:2-{5-[4-(4-isopropyl-piperazin-1-ylmethyl)-phenyl]-[2,2';4',3'']terpyridin-6'-yl}-propan-2-ol

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Chemical Property of 2-{5-[4-(4-isopropyl-piperazin-1-ylmethyl)-phenyl]-[2,2';4',3'']terpyridin-6'-yl}-propan-2-ol

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Technology Process of 2-{5-[4-(4-isopropyl-piperazin-1-ylmethyl)-phenyl]-[2,2';4',3'']terpyridin-6'-yl}-propan-2-ol

There total 3 articles about 2-{5-[4-(4-isopropyl-piperazin-1-ylmethyl)-phenyl]-[2,2';4',3'']terpyridin-6'-yl}-propan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1171045-42-3
4-((4-isopropyl-piperazin-l1yl)methyl)-phenyl boronic acid

: 1171043-73-4
2-(5-bromo-[2,2';4',3]terpyridin-6'-yl)-propan-2-ol

: 1171041-31-8
2-{5-[4-(4-isopropyl-piperazin-1-ylmethyl)-phenyl]-[2,2';4',3'']terpyridin-6'-yl}-propan-2-ol

Guidance literature:: With sodium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,2-dimethoxyethane; at 95 ℃; Microwave radiation;

Reference yield:

: 921936-97-2
N-[1-(pyridin-2-yl)ethylidene]diphenylphosphinic amide

: 1171041-31-8
2-{5-[4-(4-isopropyl-piperazin-1-ylmethyl)-phenyl]-[2,2';4',3'']terpyridin-6'-yl}-propan-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere of nitrogen

2: sodium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,2-dimethoxyethane / 95 °C / Microwave radiation

With potassium tert-butylate; sodium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,2-dimethoxyethane; N,N-dimethyl-formamide;

Reference yield:

: 1758-54-9,79462-42-3,81563-77-1
1-pyridin-2-yl-ethanone oxime

: 1171041-31-8
2-{5-[4-(4-isopropyl-piperazin-1-ylmethyl)-phenyl]-[2,2';4',3'']terpyridin-6'-yl}-propan-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / diethyl ether; dichloromethane / -40 - 20 °C / Inert atmosphere of nitrogen

2: potassium tert-butylate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere of nitrogen

3: sodium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,2-dimethoxyethane / 95 °C / Microwave radiation

With potassium tert-butylate; sodium carbonate; triethylamine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,2-dimethoxyethane; diethyl ether; dichloromethane; N,N-dimethyl-formamide;