(E)-tert-butyl (4-(2-(6-methoxybenzofuran-2-yl)vinyl)phenyl)(methyl)carbamate

Base Information

Chemical Name:(E)-tert-butyl (4-(2-(6-methoxybenzofuran-2-yl)vinyl)phenyl)(methyl)carbamate
CAS No.:1089682-48-3
Molecular Formula:C₂₃H₂₅NO₄
Molecular Weight:379.456
Hs Code.:

Synonyms:(E)-tert-butyl (4-(2-(6-methoxybenzofuran-2-yl)vinyl)phenyl)(methyl)carbamate

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Chemical Property of (E)-tert-butyl (4-(2-(6-methoxybenzofuran-2-yl)vinyl)phenyl)(methyl)carbamate

Chemical Property:

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Technology Process of (E)-tert-butyl (4-(2-(6-methoxybenzofuran-2-yl)vinyl)phenyl)(methyl)carbamate

There total 9 articles about (E)-tert-butyl (4-(2-(6-methoxybenzofuran-2-yl)vinyl)phenyl)(methyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1462470-22-9
((6-methoxybenzofuran-2-yl)methyl)triphenylphosphonium bromide

: 780821-17-2
(4-formylphenyl)(methyl)carbamic acid tert-butyl ester

: 1089682-48-3
(E)-tert-butyl (4-(2-(6-methoxybenzofuran-2-yl)vinyl)phenyl)(methyl)carbamate

Guidance literature:: (4-formylphenyl)(methyl)carbamic acid tert-butyl ester; With sodium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃; for 2h;

((6-methoxybenzofuran-2-yl)methyl)triphenylphosphonium bromide; In tetrahydrofuran; at 20 ℃; for 4.5h;

Reference yield:

: 10541-83-0,937737-33-2
N-methyl-p-aminobenzoic acid

: 1089682-48-3
(E)-tert-butyl (4-(2-(6-methoxybenzofuran-2-yl)vinyl)phenyl)(methyl)carbamate

Guidance literature:: Multi-step reaction with 5 steps

1.1: acetyl chloride / 20 h / Reflux

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 8 h / 0 °C

3.1: water; 1,4-dioxane / 16 h / 20 °C

4.1: sulfur trioxide pyridine complex; triethylamine; dimethyl sulfoxide / 3 h / 0 - 20 °C

5.1: sodium hexamethyldisilazane / tetrahydrofuran / 2 h / 0 °C

5.2: 4.5 h / 20 °C

With lithium aluminium tetrahydride; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; acetyl chloride; In tetrahydrofuran; 1,4-dioxane; water;

Reference yield:

: 181819-75-0
(4-(methylamino)phenyl)methanol

: 1089682-48-3
(E)-tert-butyl (4-(2-(6-methoxybenzofuran-2-yl)vinyl)phenyl)(methyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: water; 1,4-dioxane / 16 h / 20 °C

2.1: sulfur trioxide pyridine complex; triethylamine; dimethyl sulfoxide / 3 h / 0 - 20 °C

3.1: sodium hexamethyldisilazane / tetrahydrofuran / 2 h / 0 °C

3.2: 4.5 h / 20 °C

With sodium hexamethyldisilazane; sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; 1,4-dioxane; water;