Technology Process of C34H34N6O6S4
There total 14 articles about C34H34N6O6S4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C35H36N6O6S4;
With
lithium hydroxide;
In
methanol; dichloromethane;
at 20 ℃;
for 8h;
In
methanol; dichloromethane; water;
pH=1;
Acidic conditions;
DOI:10.1016/j.tetlet.2012.05.105
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere
1.2: 3 h / 0 °C / Inert atmosphere
2.1: ammonium hydroxide / methanol; water / 20 °C / Sonication
3.1: Lawessons reagent / benzene / 5 h / Inert atmosphere; Reflux
4.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere
4.2: 3 h / 0 °C / Inert atmosphere
4.3: 3 h / 20 °C / Inert atmosphere
5.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C
5.2: pH 1 / Acidic conditions
With
Lawessons reagent; ammonium hydroxide; potassium hydrogencarbonate; lithium hydroxide;
In
methanol; 1,2-dimethoxyethane; dichloromethane; water; benzene;
1.1: Hantzsch thiazole synthesis / 1.2: Hantzsch thiazole synthesis / 4.1: Hantzsch thiazole synthesis / 4.2: Hantzsch thiazole synthesis / 4.3: Hantzsch thiazole synthesis;
DOI:10.1016/j.tetlet.2012.05.105
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: ammonium hydroxide / methanol; water / 20 °C / Sonication
2.1: Lawessons reagent / benzene / 5 h / Inert atmosphere; Reflux
3.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere
3.2: 3 h / 0 °C / Inert atmosphere
3.3: 3 h / 20 °C / Inert atmosphere
4.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C
4.2: pH 1 / Acidic conditions
With
Lawessons reagent; ammonium hydroxide; potassium hydrogencarbonate; lithium hydroxide;
In
methanol; 1,2-dimethoxyethane; dichloromethane; water; benzene;
3.1: Hantzsch thiazole synthesis / 3.2: Hantzsch thiazole synthesis / 3.3: Hantzsch thiazole synthesis;
DOI:10.1016/j.tetlet.2012.05.105