methyl 2-(4-(2-(2-acetamidophenyl)-2-oxoacetamido)benzamido)-2-methylpropanoate

Base Information

Chemical Name:methyl 2-(4-(2-(2-acetamidophenyl)-2-oxoacetamido)benzamido)-2-methylpropanoate
CAS No.:1622349-76-1
Molecular Formula:C₂₂H₂₃N₃O₆
Molecular Weight:425.441
Hs Code.:

Synonyms:methyl 2-(4-(2-(2-acetamidophenyl)-2-oxoacetamido)benzamido)-2-methylpropanoate

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Chemical Property of methyl 2-(4-(2-(2-acetamidophenyl)-2-oxoacetamido)benzamido)-2-methylpropanoate

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Technology Process of methyl 2-(4-(2-(2-acetamidophenyl)-2-oxoacetamido)benzamido)-2-methylpropanoate

There total 5 articles about methyl 2-(4-(2-(2-acetamidophenyl)-2-oxoacetamido)benzamido)-2-methylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 702669-44-1
4-(2-(2-acetamidophenyl)-2-oxoacetamido)benzoic acid

: 15028-41-8
methyl 2-aminoisobutyrate hydrochloride

: 1622349-76-1
methyl 2-(4-(2-(2-acetamidophenyl)-2-oxoacetamido)benzamido)-2-methylpropanoate

Guidance literature:: 4-(2-(2-acetamidophenyl)-2-oxoacetamido)benzoic acid; With ethyl cyanoglyoxylate-2-oxime; diisopropyl-carbodiimide; In N,N-dimethyl-formamide; at 0 ℃; for 0.0833333h;

methyl 2-aminoisobutyrate hydrochloride; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 ℃; for 1h;
DOI:10.3390/molecules181214747

Reference yield: 76.0%

: 13257-67-5
2-amino-2-methylpropionic acid methyl ester

: 702669-44-1
4-(2-(2-acetamidophenyl)-2-oxoacetamido)benzoic acid

: 1622349-76-1
methyl 2-(4-(2-(2-acetamidophenyl)-2-oxoacetamido)benzamido)-2-methylpropanoate

Guidance literature:: 4-(2-(2-acetamidophenyl)-2-oxoacetamido)benzoic acid; With ethyl cyanoglyoxylate-2-oxime; diisopropyl-carbodiimide; In N,N-dimethyl-formamide; at 0 ℃; for 0.0833333h;

2-amino-2-methylpropionic acid methyl ester; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1016/j.bmcl.2014.11.007

Reference yield:

: 574-17-4
1-acetyl-1H-indole-2,3-dione

: 1622349-76-1
methyl 2-(4-(2-(2-acetamidophenyl)-2-oxoacetamido)benzamido)-2-methylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanol / 0.07 h / 80 °C / 150.01 Torr / Sealed tube

2.1: ethyl cyanoglyoxylate-2-oxime; diisopropyl-carbodiimide / N,N-dimethyl-formamide / 0.08 h / 0 °C

2.2: 1 h / 0 °C

With ethyl cyanoglyoxylate-2-oxime; diisopropyl-carbodiimide; In methanol; N,N-dimethyl-formamide;
DOI:10.3390/molecules181214747