((2-Acetoxy-benzyl)-{2-[(2-acetoxy-benzyl)-tert-butoxycarbonylmethyl-amino]-ethyl}-amino)-acetic acid tert-butyl ester

Base Information

Chemical Name:((2-Acetoxy-benzyl)-{2-[(2-acetoxy-benzyl)-tert-butoxycarbonylmethyl-amino]-ethyl}-amino)-acetic acid tert-butyl ester
CAS No.:102212-17-9
Molecular Formula:C₃₂H₄₄N₂O₈
Molecular Weight:584.71
Hs Code.:

Synonyms:((2-Acetoxy-benzyl)-{2-[(2-acetoxy-benzyl)-tert-butoxycarbonylmethyl-amino]-ethyl}-amino)-acetic acid tert-butyl ester

Suppliers and Price of ((2-Acetoxy-benzyl)-{2-[(2-acetoxy-benzyl)-tert-butoxycarbonylmethyl-amino]-ethyl}-amino)-acetic acid tert-butyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ((2-Acetoxy-benzyl)-{2-[(2-acetoxy-benzyl)-tert-butoxycarbonylmethyl-amino]-ethyl}-amino)-acetic acid tert-butyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ((2-Acetoxy-benzyl)-{2-[(2-acetoxy-benzyl)-tert-butoxycarbonylmethyl-amino]-ethyl}-amino)-acetic acid tert-butyl ester

There total 4 articles about ((2-Acetoxy-benzyl)-{2-[(2-acetoxy-benzyl)-tert-butoxycarbonylmethyl-amino]-ethyl}-amino)-acetic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 704-65-4
2-(bromomethyl)phenyl acetate

: 102212-16-8
di-tert-butyl 2,2’-(ethane-1,2-diylbis(azanediyl))diacetate

: 102212-17-9
((2-Acetoxy-benzyl)-{2-[(2-acetoxy-benzyl)-tert-butoxycarbonylmethyl-amino]-ethyl}-amino)-acetic acid tert-butyl ester

Guidance literature:: With potassium carbonate; In acetone; for 10h; Heating;
DOI:10.1021/jm00157a020

Reference yield:

: 5657-17-0
ethylenediaminediacetic acid

: 102212-17-9
((2-Acetoxy-benzyl)-{2-[(2-acetoxy-benzyl)-tert-butoxycarbonylmethyl-amino]-ethyl}-amino)-acetic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / sodium bicarbonate / diethyl ether; H₂O

2: 7.0 g / H₂SO₄ / CH₂Cl₂ / 96 h / Ambient temperature

3: 3.6 g / H₂ / 10percent Pd/C / ethanol / 72 h

4: 42 percent / K₂CO₃ / acetone / 10 h / Heating

With sulfuric acid; hydrogen; sodium hydrogencarbonate; potassium carbonate; palladium on activated charcoal; In diethyl ether; ethanol; dichloromethane; water; acetone;
DOI:10.1021/jm00157a020

Reference yield:

: 102212-15-7
N,N'-bis(benzyloxycarbonyl)ethylenediamine-N,N'-diacetic acid

: 102212-17-9
((2-Acetoxy-benzyl)-{2-[(2-acetoxy-benzyl)-tert-butoxycarbonylmethyl-amino]-ethyl}-amino)-acetic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 7.0 g / H₂SO₄ / CH₂Cl₂ / 96 h / Ambient temperature

2: 3.6 g / H₂ / 10percent Pd/C / ethanol / 72 h

3: 42 percent / K₂CO₃ / acetone / 10 h / Heating

With sulfuric acid; hydrogen; potassium carbonate; palladium on activated charcoal; In ethanol; dichloromethane; acetone;
DOI:10.1021/jm00157a020