methyl 2,3,4-tri-O-benzyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Base Information

Chemical Name:methyl 2,3,4-tri-O-benzyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside
CAS No.:76679-49-7
Molecular Formula:C₅₅H₆₀O₁₁
Molecular Weight:897.075
Hs Code.:

Synonyms:methyl 2,3,4-tri-O-benzyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

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Chemical Property of methyl 2,3,4-tri-O-benzyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

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Technology Process of methyl 2,3,4-tri-O-benzyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

There total 5 articles about methyl 2,3,4-tri-O-benzyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1200763-23-0
methyl 2,3,4-tri-O-benzyl-6-O-(2',3',4'-tri-O-benzyl-6'-O-levulinoyl-β-D-glucopyranosyl)-1-α-D-glucopyranoside

: 76679-49-7
methyl 2,3,4-tri-O-benzyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: With sodium; In methanol; dichloromethane; at 20 ℃;
DOI:10.1002/chem.200901119

Reference yield: 89.0%

: 1415590-78-1
methyl O-(2,3,4-tri-O-benzyl-6-O-picoloyl-β-D-glucopyranosyl)-(1→6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: 76679-49-7
methyl 2,3,4-tri-O-benzyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: With copper diacetate; In methanol; dichloromethane; at 20 ℃; for 3h; chemoselective reaction;
DOI:10.1021/acs.orglett.5b02110

Reference yield:

: 87470-73-3,120403-26-1,38184-12-2
phenyl 2,3,4-tri-O-benzyl-1-thio-β-D-glucopyranoside

: 76679-49-7
methyl 2,3,4-tri-O-benzyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 0.25 h / 20 °C / Inert atmosphere

2.1: palladium(II) bromide / dichloromethane / 3 h / 20 °C / Molecular sieve; Inert atmosphere

2.2: 8 h / -30 - 20 °C / Inert atmosphere

2.3: 0.5 h / 20 °C / Inert atmosphere

3.1: copper diacetate / dichloromethane; methanol / 3 h / 20 °C

With dmap; copper diacetate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium(II) bromide; In methanol; dichloromethane;
DOI:10.1021/acs.orglett.5b02110