1-(2-O-acetyl-3,4-O-isopropylidene-α-D-arabinopyranosyl)-N4-benzoylcytosine

Base Information

Chemical Name:1-(2-O-acetyl-3,4-O-isopropylidene-α-D-arabinopyranosyl)-N4-benzoylcytosine
CAS No.:1293285-47-8
Molecular Formula:C₂₁H₂₃N₃O₇
Molecular Weight:429.43
Hs Code.:

Synonyms:1-(2-O-acetyl-3,4-O-isopropylidene-α-D-arabinopyranosyl)-N4-benzoylcytosine

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Chemical Property of 1-(2-O-acetyl-3,4-O-isopropylidene-α-D-arabinopyranosyl)-N4-benzoylcytosine

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Technology Process of 1-(2-O-acetyl-3,4-O-isopropylidene-α-D-arabinopyranosyl)-N4-benzoylcytosine

There total 5 articles about 1-(2-O-acetyl-3,4-O-isopropylidene-α-D-arabinopyranosyl)-N4-benzoylcytosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1293285-39-8
C₁₉H₂₁N₃O₆

: 108-24-7
acetic anhydride

: 1293285-47-8
1-(2-O-acetyl-3,4-O-isopropylidene-α-D-arabinopyranosyl)-N4-benzoylcytosine

Guidance literature:: With pyridine; at 4 ℃;
DOI:10.1016/j.ejmech.2011.01.005

Reference yield:

: 1293285-30-9
1-(α-D-arabinopyranosyl)-N4-benzoylcytosine

: 1293285-47-8
1-(2-O-acetyl-3,4-O-isopropylidene-α-D-arabinopyranosyl)-N4-benzoylcytosine

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / acetone / 6 h

2: pyridine / 4 °C

With pyridine; toluene-4-sulfonic acid; In acetone;
DOI:10.1016/j.ejmech.2011.01.005

Reference yield:

: 1293285-24-1
1-(2,3,4-tri-O-acetyl-α-D-arabinopyranosyl)-N4-benzoylcytosine

: 1293285-47-8
1-(2-O-acetyl-3,4-O-isopropylidene-α-D-arabinopyranosyl)-N4-benzoylcytosine

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; ethanol; sodium hydroxide / 0.18 h / 20 °C

2: toluene-4-sulfonic acid / acetone / 6 h

3: pyridine / 4 °C

With pyridine; ethanol; toluene-4-sulfonic acid; sodium hydroxide; In acetone;
DOI:10.1016/j.ejmech.2011.01.005