tricarbonyl(η4:2-7,8-diphenyl-9-N-cyano-9-azabicyclo[4.2.1]-nona-2,4,7-triene)-chromium(0)

Base Information

Chemical Name:tricarbonyl(η4:2-7,8-diphenyl-9-N-cyano-9-azabicyclo[4.2.1]-nona-2,4,7-triene)-chromium(0)
CAS No.:460719-09-9
Molecular Formula:C₂₄H₁₆CrN₂O₃
Molecular Weight:432.399
Hs Code.:

Synonyms:tricarbonyl(η4:2-7,8-diphenyl-9-N-cyano-9-azabicyclo[4.2.1]-nona-2,4,7-triene)-chromium(0)

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Chemical Property of tricarbonyl(η4:2-7,8-diphenyl-9-N-cyano-9-azabicyclo[4.2.1]-nona-2,4,7-triene)-chromium(0)

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Technology Process of tricarbonyl(η4:2-7,8-diphenyl-9-N-cyano-9-azabicyclo[4.2.1]-nona-2,4,7-triene)-chromium(0)

There total 1 articles about tricarbonyl(η4:2-7,8-diphenyl-9-N-cyano-9-azabicyclo[4.2.1]-nona-2,4,7-triene)-chromium(0) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 460719-06-6
tricarbonyl(η6-N-cyanoazepine)chromium(0)

: 501-65-5
diphenyl acetylene

: 460719-09-9
tricarbonyl(η4:2-7,8-diphenyl-9-N-cyano-9-azabicyclo[4.2.1]-nona-2,4,7-triene)-chromium(0)

Guidance literature:: In toluene; Irradiation (UV/VIS); (N2); irradiation of a soln. of metal complex and alkyne in toluene withHg lamp at 263 K for 540 min; filtration through Celite, evapn., recrystn. (n-hexane/CH2Cl2, 5:1); elem. anal.;
DOI:10.1016/S0022-328X(02)01369-4

Reference yield: 75.0%

: 460719-09-9
tricarbonyl(η4:2-7,8-diphenyl-9-N-cyano-9-azabicyclo[4.2.1]-nona-2,4,7-triene)-chromium(0)

: 12083-24-8
tricarbonyl(η(6)-toluene)chromium

: 7,8-diphenyl-9-N-cyano-9-azabicyclo[4.2.1]-nona-2,4,7-triene

Guidance literature:: In toluene; (N2); refluxing a soln. of chromium complex in toluene for 10 min; evapn., thin layer chromy. (SiO2, hexane/CH2Cl2 1:1); elem. anal.;
DOI:10.1016/S0022-328X(02)01369-4