C₃₃H₄₈N₄O₄

Base Information

Chemical Name:C₃₃H₄₈N₄O₄
CAS No.:1561902-67-7
Molecular Formula:C₃₃H₄₈N₄O₄
Molecular Weight:564.769
Hs Code.:

C<sub>33</sub>H<sub>48</sub>N<sub>4</sub>O<sub>4</sub>

Synonyms:C₃₃H₄₈N₄O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₄₈N₄O₄

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Technology Process of C₃₃H₄₈N₄O₄

There total 12 articles about C₃₃H₄₈N₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1561902-66-6
C₃₃H₄₄N₄O₈

: 1561902-67-7
C₃₃H₄₈N₄O₄

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethyl acetate; at 20 ℃; for 16h; under 2625.26 Torr;
DOI:10.1039/c3ob42309c

Reference yield:

: 947-04-6,25038-74-8
2-azacyclotridecanone

: 1561902-67-7
C₃₃H₄₈N₄O₄

Guidance literature:: Multi-step reaction with 6 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere; Reflux

2: triethylamine / N,N-dimethyl-formamide / 16 h / 70 °C / Inert atmosphere

3: lithium aluminium tetrahydride / diethyl ether / 0.25 h / 0 - 33 °C / Inert atmosphere

4: sodium iodide / dimethyl sulfoxide / 0.25 h / 20 °C / Inert atmosphere

5: methanol / 16 h / 20 °C

6: palladium 10% on activated carbon; hydrogen / ethyl acetate / 16 h / 20 °C / 2625.26 Torr

With lithium aluminium tetrahydride; palladium 10% on activated carbon; hydrogen; triethylamine; sodium iodide; In tetrahydrofuran; methanol; diethyl ether; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1039/c3ob42309c

Reference yield:

: 295-03-4
azacyclotridecane

: 1561902-67-7
C₃₃H₄₈N₄O₄

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / N,N-dimethyl-formamide / 16 h / 70 °C / Inert atmosphere

2: lithium aluminium tetrahydride / diethyl ether / 0.25 h / 0 - 33 °C / Inert atmosphere

3: sodium iodide / dimethyl sulfoxide / 0.25 h / 20 °C / Inert atmosphere

4: methanol / 16 h / 20 °C

5: palladium 10% on activated carbon; hydrogen / ethyl acetate / 16 h / 20 °C / 2625.26 Torr

With lithium aluminium tetrahydride; palladium 10% on activated carbon; hydrogen; triethylamine; sodium iodide; In methanol; diethyl ether; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1039/c3ob42309c