8-[4-({[({2-[({4-[(tert-butyloxycarbonyl)amino]phenyl}acetyl)amino]ethyl}amino)carbonyl]methyl}oxy)phenyl]-1,3-dipropylxanthine

Base Information

Chemical Name:8-[4-({[({2-[({4-[(tert-butyloxycarbonyl)amino]phenyl}acetyl)amino]ethyl}amino)carbonyl]methyl}oxy)phenyl]-1,3-dipropylxanthine
CAS No.:120059-13-4
Molecular Formula:C₃₄H₄₃N₇O₇
Molecular Weight:661.758
Hs Code.:

Synonyms:8-[4-({[({2-[({4-[(tert-butyloxycarbonyl)amino]phenyl}acetyl)amino]ethyl}amino)carbonyl]methyl}oxy)phenyl]-1,3-dipropylxanthine

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Chemical Property of 8-[4-({[({2-[({4-[(tert-butyloxycarbonyl)amino]phenyl}acetyl)amino]ethyl}amino)carbonyl]methyl}oxy)phenyl]-1,3-dipropylxanthine

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Technology Process of 8-[4-({[({2-[({4-[(tert-butyloxycarbonyl)amino]phenyl}acetyl)amino]ethyl}amino)carbonyl]methyl}oxy)phenyl]-1,3-dipropylxanthine

There total 4 articles about 8-[4-({[({2-[({4-[(tert-butyloxycarbonyl)amino]phenyl}acetyl)amino]ethyl}amino)carbonyl]methyl}oxy)phenyl]-1,3-dipropylxanthine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 96865-92-8
xanthine amine congener

: 120059-12-3
N-Succinimidyl 4-<(tert-butyloxycarbonyl)amino>phenylacetate

: 120059-13-4
8-[4-({[({2-[({4-[(tert-butyloxycarbonyl)amino]phenyl}acetyl)amino]ethyl}amino)carbonyl]methyl}oxy)phenyl]-1,3-dipropylxanthine

Guidance literature:: In N,N-dimethyl-formamide; for 2h;
DOI:10.1021/jm00125a019

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 120059-13-4
8-[4-({[({2-[({4-[(tert-butyloxycarbonyl)amino]phenyl}acetyl)amino]ethyl}amino)carbonyl]methyl}oxy)phenyl]-1,3-dipropylxanthine

Guidance literature:: Multi-step reaction with 3 steps

1: 40 percent / Na₂HPO₄ / methanol; H₂O / 2 h

2: 69 percent / 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide*HCl / dimethylformamide / 2 h

3: 75 percent / dimethylformamide / 2 h

With disodium hydrogenphosphate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00125a019

Reference yield:

: 1197-55-3
4-aminophenylacetic acid

: 120059-13-4
8-[4-({[({2-[({4-[(tert-butyloxycarbonyl)amino]phenyl}acetyl)amino]ethyl}amino)carbonyl]methyl}oxy)phenyl]-1,3-dipropylxanthine

Guidance literature:: Multi-step reaction with 3 steps

1: 40 percent / Na₂HPO₄ / methanol; H₂O / 2 h

2: 69 percent / 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide*HCl / dimethylformamide / 2 h

3: 75 percent / dimethylformamide / 2 h

With disodium hydrogenphosphate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00125a019