O,O-dimethyl [2-(4,6-dimethoxypyrimidin-2-yloxy)phenoxyamino](4-chlorophenyl)methylphosphonate

Base Information

Chemical Name:O,O-dimethyl [2-(4,6-dimethoxypyrimidin-2-yloxy)phenoxyamino](4-chlorophenyl)methylphosphonate
CAS No.:1347739-90-5
Molecular Formula:C₂₂H₂₃ClN₃O₇P
Molecular Weight:507.867
Hs Code.:

Synonyms:O,O-dimethyl [2-(4,6-dimethoxypyrimidin-2-yloxy)phenoxyamino](4-chlorophenyl)methylphosphonate

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Chemical Property of O,O-dimethyl [2-(4,6-dimethoxypyrimidin-2-yloxy)phenoxyamino](4-chlorophenyl)methylphosphonate

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Technology Process of O,O-dimethyl [2-(4,6-dimethoxypyrimidin-2-yloxy)phenoxyamino](4-chlorophenyl)methylphosphonate

There total 8 articles about O,O-dimethyl [2-(4,6-dimethoxypyrimidin-2-yloxy)phenoxyamino](4-chlorophenyl)methylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 110284-78-1
2-(4',6'-dimethoxypyrimidine-2'-yl)oxy-benzoic acid

: [amino-(4-chloro-phenyl)-methyl]-phosphonic acid dimethyl ester

: 1347739-90-5
O,O-dimethyl [2-(4,6-dimethoxypyrimidin-2-yloxy)phenoxyamino](4-chlorophenyl)methylphosphonate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 25 ℃;
DOI:10.1080/10426507.2011.558363

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 1347739-90-5
O,O-dimethyl [2-(4,6-dimethoxypyrimidin-2-yloxy)phenoxyamino](4-chlorophenyl)methylphosphonate

Guidance literature:: Multi-step reaction with 5 steps

1: ammonium hydroxide / water / 5 h / Reflux

2: 70 °C

3: tetrahydrofuran / 2 h / 0 °C

4: ammonium hydroxide / water / 0.5 h / 20 °C

5: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 25 °C

With dmap; ammonium hydroxide; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1080/10426507.2011.558363

Reference yield:

: C₇H₈O₃S*C₉H₁₃ClNO₃P

: 1347739-90-5
O,O-dimethyl [2-(4,6-dimethoxypyrimidin-2-yloxy)phenoxyamino](4-chlorophenyl)methylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium hydroxide / water / 0.5 h / 20 °C

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 25 °C

With dmap; ammonium hydroxide; dicyclohexyl-carbodiimide; In dichloromethane; water;
DOI:10.1080/10426507.2011.558363