N,N-dioctadecylaniline

Base Information

Chemical Name:N,N-dioctadecylaniline
CAS No.:72072-19-6
Molecular Formula:C₄₂H₇₉N
Molecular Weight:598.096
Hs Code.:
European Community (EC) Number:660-821-0
Nikkaji Number:J852.378I
ChEMBL ID:CHEMBL1884790
Mol file:72072-19-6.mol

Synonyms:N,N-dioctadecylaniline;72072-19-6;N-dioctadecylaniline;N,N-dioctadecyl-N-phenylamine;SCHEMBL639797;CHEMBL1884790;AMY6942;JDEDKRLRGDEWKM-UHFFFAOYSA-N;AKOS024434104;NCGC00188199-01;NCGC00188199-02

Suppliers and Price of N,N-dioctadecylaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
N,N-DIOCTADECYLANILINE Aldrich
1ea
$ 144.00

Crysdot
N,N-Dioctadecylaniline 97%
5g
$ 900.00

Crysdot
N,N-Dioctadecylaniline 97%
1g
$ 300.00

Alichem
N,N-Dioctadecylaniline
5g
$ 954.00

Total 15 raw suppliers

Chemical Property of N,N-dioctadecylaniline

Chemical Property:

Melting Point:40-41 °C
Boiling Point:652.3±24.0 °C(Predicted)
PKA:6.28±0.50(Predicted)
Density:0.868±0.06 g/cm3(Predicted)
XLogP3:19.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:35
Exact Mass:597.62125152
Heavy Atom Count:43
Complexity:459

Purity/Quality:

99% ^*data from raw suppliers

N,N-DIOCTADECYLANILINE Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCCCCCCCCCCCCCN(CCCCCCCCCCCCCCCCCC)C1=CC=CC=C1

Technology Process of N,N-dioctadecylaniline

There total 7 articles about N,N-dioctadecylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.31%

: 62-53-3
aniline

: 112-89-0
1-Bromooctadecane

: 72072-19-6
N,N-di(octadecyl)aniline

Guidance literature:: With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate; In N,N-dimethyl-formamide; at 115 ℃; for 15h; Reagent/catalyst; Autoclave; Inert atmosphere; Large scale;

Reference yield:

: 3386-32-1
n-octadecyl p-toluenesulfonate

: 62-53-3
aniline

: 25417-58-7
N-octadecylbenzeneamine

: 72072-19-6
N,N-di(octadecyl)aniline

Guidance literature:: With sodium carbonate;
DOI:10.1021/jo01132a005

Reference yield:

: 112-99-2
Dioctadecylamine

: 72072-19-6
N,N-di(octadecyl)aniline

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / 1-methyl-2-pyrrolidinone (NMP), triethylamine / 100 °C

2: 89 percent / SnCl₂*2H₂O, Sn, conc. HCl / toluene; ethanol / Heating

3: 1.) H₃PO₂, NaNO₂, 2.) aq. NaOH / 1.) a) ethanol, 0 deg C, 30 min, b) RT, overnight

With 1-methyl-pyrrolidin-2-one; hydrogenchloride; sodium hydroxide; tin; hypophosphorous acid; triethylamine; tin(ll) chloride; sodium nitrite; In ethanol; toluene;
DOI:10.1021/jo00258a027