{5-[4'-(1-methanesulfonylaminocarbonyl-cyclopropyl)biphenyl-4-yl]-3-methyl-3H-[1,2,3]triazol-4-yl}carbamic acid (R)-1-phenyl-ethyl ester

Base Information

Chemical Name:{5-[4'-(1-methanesulfonylaminocarbonyl-cyclopropyl)biphenyl-4-yl]-3-methyl-3H-[1,2,3]triazol-4-yl}carbamic acid (R)-1-phenyl-ethyl ester
CAS No.:1396007-78-5
Molecular Formula:C₂₉H₂₉N₅O₅S
Molecular Weight:559.646
Hs Code.:

Synonyms:{5-[4'-(1-methanesulfonylaminocarbonyl-cyclopropyl)biphenyl-4-yl]-3-methyl-3H-[1,2,3]triazol-4-yl}carbamic acid (R)-1-phenyl-ethyl ester

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Chemical Property of {5-[4'-(1-methanesulfonylaminocarbonyl-cyclopropyl)biphenyl-4-yl]-3-methyl-3H-[1,2,3]triazol-4-yl}carbamic acid (R)-1-phenyl-ethyl ester

Chemical Property:

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Technology Process of {5-[4'-(1-methanesulfonylaminocarbonyl-cyclopropyl)biphenyl-4-yl]-3-methyl-3H-[1,2,3]triazol-4-yl}carbamic acid (R)-1-phenyl-ethyl ester

There total 10 articles about {5-[4'-(1-methanesulfonylaminocarbonyl-cyclopropyl)biphenyl-4-yl]-3-methyl-3H-[1,2,3]triazol-4-yl}carbamic acid (R)-1-phenyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1257214-59-7
N-{1-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-cyclopropanecarbonyl}-methanesulfonamide

: 1396008-13-1
[5-(4-bromo-phenyl)-3-methyl-3H-[1,2,3]triazol-4-yl]carbamic acid (R)-1-phenyl-ethyl ester

: 1396007-78-5
{5-[4'-(1-methanesulfonylaminocarbonyl-cyclopropyl)biphenyl-4-yl]-3-methyl-3H-[1,2,3]triazol-4-yl}carbamic acid (R)-1-phenyl-ethyl ester

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 4h; Inert atmosphere; Sealed tube;

Reference yield:

: 1257214-56-4
N-[1-(4-bromo-phenyl)-cyclopropanecarbonyl]-methanesulfonamide

: 1396007-78-5
{5-[4'-(1-methanesulfonylaminocarbonyl-cyclopropyl)biphenyl-4-yl]-3-methyl-3H-[1,2,3]triazol-4-yl}carbamic acid (R)-1-phenyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 16 h / 80 °C / Inert atmosphere; Sealed tube

2: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; 1,1'-bis-(diphenylphosphino)ferrocene; sodium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C / Inert atmosphere; Sealed tube

With 1,1'-bis-(diphenylphosphino)ferrocene; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; sodium carbonate; In 1,4-dioxane; N,N-dimethyl-formamide;

Reference yield:

: 1-(4-bromophenyl)cyclopropanoyl chloride

: 1396007-78-5
{5-[4'-(1-methanesulfonylaminocarbonyl-cyclopropyl)biphenyl-4-yl]-3-methyl-3H-[1,2,3]triazol-4-yl}carbamic acid (R)-1-phenyl-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 20 °C / Inert atmosphere; Cooling with ice

1.2: 20 °C / Inert atmosphere; Cooling with ice

2.1: potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 16 h / 80 °C / Inert atmosphere; Sealed tube

3.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; 1,1'-bis-(diphenylphosphino)ferrocene; sodium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C / Inert atmosphere; Sealed tube

With 1,1'-bis-(diphenylphosphino)ferrocene; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; sodium hydride; sodium carbonate; In 1,4-dioxane; N,N-dimethyl-formamide;