A₁₂

Base Information

Chemical Name:A₁₂
CAS No.:1592908-16-1
Molecular Formula:C₃₆H₃₈BrN₃O₆
Molecular Weight:688.618
Hs Code.:

Synonyms:A₁₂

Suppliers and Price of A₁₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of A₁₂

Chemical Property:

Boiling Point:860.2±65.0 °C(Predicted)
Density:1.39±0.1 g/cm3(Predicted)

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of A₁₂

There total 11 articles about A₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: C₄₁H₅₀BrN₃O₆Si

: 1592908-16-1
A₁₂

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/ejoc.201301769

Reference yield: 93.0%

: C₄₂H₅₀BrN₃O₈Si

: 1592908-16-1
A₁₂

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/ejoc.201301769

Reference yield:

: 958138-35-7
C₁₅H₂₁NO₆

: 1592908-16-1
A₁₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 0 °C / Inert atmosphere

2.1: lithium borohydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3.1: triphenylphosphine; diethylazodicarboxylate; diphenyl phosphoryl azide / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere

4.1: water; triphenylphosphine / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

5.1: pyridine / dichloromethane / 2 h / 0 °C / Inert atmosphere

5.2: 2.08 h / 0 °C / Inert atmosphere

6.1: morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 1 h / 0 °C / Inert atmosphere; Darkness

7.1: acetic acid; sodium cyanoborohydride / ethanol / 4 h / 20 °C / Inert atmosphere

8.1: N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate / dichloromethane / 20 °C / Inert atmosphere

9.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With morpholine; pyridine; lithium borohydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diphenyl phosphoryl azide; tetrabutyl ammonium fluoride; water; sodium cyanoborohydride; acetic acid; N-ethyl-N,N-diisopropylamine; triphenylphosphine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; diethylazodicarboxylate; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1002/ejoc.201301769