4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyl bromide

Base Information

• Chemical Name: 4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyl bromide
• CAS No.: 1356472-34-8
• Molecular Formula: C₂₇H₂₉BrO₆
• Molecular Weight: 529.428

Synonyms:4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyl bromide

Chemical Property of 4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyl bromide

Chemical Property:

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Technology Process of 4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyl bromide

There total 1 articles about 4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyl alcohol (1356472-28-0) → 4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyl bromide (1356472-34-8)

Guidance literature:

With N-Bromosuccinimide; triphenylphosphine; In dichloromethane; at 0 ℃; for 0.166667h;

DOI:10.1039/c1nj20841a

Reference yield: 95.0%

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + 4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyl bromide (1356472-34-8) → 4-(4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyloxy)nitrobenzene (1356472-04-2)

Guidance literature:

With 18-crown-6 ether; potassium carbonate; In acetone; for 24h; Reflux;

DOI:10.1039/c1nj20841a

Reference yield: 63.0%

4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyl bromide (1356472-34-8) + vanillin (121-33-5,8014-42-4) → 4-(4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzaldehyde (1356472-23-5)

Guidance literature:

With 18-crown-6 ether; potassium carbonate; In acetone; for 48h; Reflux;

DOI:10.1039/c1nj20841a

upstream raw materials:

4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyl alcohol

Downstream raw materials:

4-(4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyloxy)nitrobenzene

2-Methoxy-4-methylphenol

4-(4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzaldehyde

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