10-(methyl(phenyl)amino)decyl acetate

Base Information

• Chemical Name: 10-(methyl(phenyl)amino)decyl acetate
• CAS No.: 1259289-90-1
• Molecular Formula: C₁₉H₃₁NO₂
• Molecular Weight: 305.461
• Mol file: 1259289-90-1.mol

Synonyms:10-(methyl(phenyl)amino)decyl acetate

Chemical Property of 10-(methyl(phenyl)amino)decyl acetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 10-(methyl(phenyl)amino)decyl acetate

There total 5 articles about 10-(methyl(phenyl)amino)decyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

acetic anhydride (108-24-7) + N-(10-hydroxydecyl)-N-methylaniline (185745-96-4) → 10-(methyl(phenyl)amino)decyl acetate (1259289-90-1)

Guidance literature:

With dmap; In dichloromethane; at 20 ℃; Inert atmosphere; Cooling with ice;

DOI:10.1016/j.tetlet.2010.10.120

Reference yield:

1-bromo-10-decanol (53463-68-6) → 10-(methyl(phenyl)amino)decyl acetate (1259289-90-1)

Guidance literature:

Multi-step reaction with 4 steps

1: toluene-4-sulfonic acid / tetrahydrofuran / 20 °C / Inert atmosphere

2: sodium hydride / tetrahydrofuran; mineral oil / Inert atmosphere; Reflux

3: hydrogenchloride; water / methanol / Reflux

4: dmap / dichloromethane / 20 °C / Inert atmosphere; Cooling with ice

With hydrogenchloride; dmap; water; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane; mineral oil;

DOI:10.1016/j.tetlet.2010.10.120

Reference yield:

1,10-Decanediol (112-47-0) → 10-(methyl(phenyl)amino)decyl acetate (1259289-90-1)

Guidance literature:

Multi-step reaction with 5 steps

1: hydrogen bromide / toluene / 72 h / Reflux; Inert atmosphere

2: toluene-4-sulfonic acid / tetrahydrofuran / 20 °C / Inert atmosphere

3: sodium hydride / tetrahydrofuran; mineral oil / Inert atmosphere; Reflux

4: hydrogenchloride; water / methanol / Reflux

5: dmap / dichloromethane / 20 °C / Inert atmosphere; Cooling with ice

With hydrogenchloride; dmap; water; hydrogen bromide; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane; toluene; mineral oil;

DOI:10.1016/j.tetlet.2010.10.120

upstream raw materials:

1,10-Decanediol

1-bromo-10-decanol

1-bromo-10-(tetrahydropyranyloxy)decane

acetic anhydride

Downstream raw materials:

4-((10-hydroxydecyl)(methyl)amino)benzaldehyde

4-(methyl(10-(tetrahydro-2H-pyran-2-yloxy)decyl)amino)benzaldehyde