3-ethynyl-2-(4-hydroxy-2,6-dimethylphenyl)-9-mesityl-[1,10]phenanthroline

Base Information

Chemical Name:3-ethynyl-2-(4-hydroxy-2,6-dimethylphenyl)-9-mesityl-[1,10]phenanthroline
CAS No.:949922-97-8
Molecular Formula:C₃₁H₂₆N₂O
Molecular Weight:442.56
Hs Code.:

Synonyms:3-ethynyl-2-(4-hydroxy-2,6-dimethylphenyl)-9-mesityl-[1,10]phenanthroline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-ethynyl-2-(4-hydroxy-2,6-dimethylphenyl)-9-mesityl-[1,10]phenanthroline

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Technology Process of 3-ethynyl-2-(4-hydroxy-2,6-dimethylphenyl)-9-mesityl-[1,10]phenanthroline

There total 1 articles about 3-ethynyl-2-(4-hydroxy-2,6-dimethylphenyl)-9-mesityl-[1,10]phenanthroline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 910212-82-7
2-[2,6-dimethyl-4-(triisopropylsilanyloxy)phenyl]-9-(2,4,6-trimethylphenyl)-3-trimethylsilanylethynyl[1,10]phenanthroline

: 949922-97-8
3-ethynyl-2-(4-hydroxy-2,6-dimethylphenyl)-9-mesityl-[1,10]phenanthroline

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 24h;
DOI:10.1039/b703633g

Reference yield: 91.0%

: 949922-97-8
3-ethynyl-2-(4-hydroxy-2,6-dimethylphenyl)-9-mesityl-[1,10]phenanthroline

: 626-44-8
1,3,5-Triiodobenzene

: 1084886-23-6
C₉₉H₇₈N₆O₃

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In N,N-dimethyl-formamide; at 60 ℃; for 4h; Inert atmosphere;
DOI:10.1039/b808988d

Reference yield: 90.0%

: 949922-97-8
3-ethynyl-2-(4-hydroxy-2,6-dimethylphenyl)-9-mesityl-[1,10]phenanthroline

: 624-38-4,1032416-46-8
para-diiodobenzene

: 864720-32-1
1,4-bis[(2-(4-hydroxy-2,6-dimethylphenyl)-9-mesityl-[1,10]phenanthroline-3-yl)ethynyl]benzene

Guidance literature:: With triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 60 ℃; for 4h;
DOI:10.1039/b703633g