1-[4-(2-Benzyloxy-3,4-dimethoxy-phenyl)-6-methoxycarbonyl-5-methyl-pyridin-2-ylmethyl]-1-cyanomethyl-pyrrolidinium; chloride

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Chemical Name:1-[4-(2-Benzyloxy-3,4-dimethoxy-phenyl)-6-methoxycarbonyl-5-methyl-pyridin-2-ylmethyl]-1-cyanomethyl-pyrrolidinium; chloride
CAS No.:79953-19-8
Molecular Formula:C₃₀H₃₄N₃O₅*Cl
Molecular Weight:552.07
Hs Code.:
Mol file:79953-19-8.mol

Synonyms:1-[4-(2-Benzyloxy-3,4-dimethoxy-phenyl)-6-methoxycarbonyl-5-methyl-pyridin-2-ylmethyl]-1-cyanomethyl-pyrrolidinium; chloride

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Chemical Property of 1-[4-(2-Benzyloxy-3,4-dimethoxy-phenyl)-6-methoxycarbonyl-5-methyl-pyridin-2-ylmethyl]-1-cyanomethyl-pyrrolidinium; chloride Edit

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Technology Process of 1-[4-(2-Benzyloxy-3,4-dimethoxy-phenyl)-6-methoxycarbonyl-5-methyl-pyridin-2-ylmethyl]-1-cyanomethyl-pyrrolidinium; chloride

There total 12 articles about 1-[4-(2-Benzyloxy-3,4-dimethoxy-phenyl)-6-methoxycarbonyl-5-methyl-pyridin-2-ylmethyl]-1-cyanomethyl-pyrrolidinium; chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74614-98-5
methyl 4-<3,4-dimethoxy-2-(phenylmethoxy)phenyl>-6-(hydroxymethyl)-3-methyl-2-pyridinecarboxylate

: 79953-19-8
1-[4-(2-Benzyloxy-3,4-dimethoxy-phenyl)-6-methoxycarbonyl-5-methyl-pyridin-2-ylmethyl]-1-cyanomethyl-pyrrolidinium; chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / thionyl chloride / benzene / 1.5 h / Ambient temperature

2: dimethylsulfoxide / 120 h / 45 °C

With thionyl chloride; In dimethyl sulfoxide; benzene;
DOI:10.1021/ja00366a028

Reference yield:

: 74614-97-4
methyl 6-<(acetyloxy)methyl>-4-<3,4-dimethoxy-2-(phenylmethoxy)phenyl>-3-methyl-2-pyridinecarboxylate

: 79953-19-8
1-[4-(2-Benzyloxy-3,4-dimethoxy-phenyl)-6-methoxycarbonyl-5-methyl-pyridin-2-ylmethyl]-1-cyanomethyl-pyrrolidinium; chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / K₂CO₃ / methanol / 2 h / Ambient temperature

2: 100 percent / thionyl chloride / benzene / 1.5 h / Ambient temperature

3: dimethylsulfoxide / 120 h / 45 °C

With thionyl chloride; potassium carbonate; In methanol; dimethyl sulfoxide; benzene;
DOI:10.1021/ja00366a028